Microscopy Morphology — Self-assembled Mo doped Ni-MOF nanosheets based electrode material for high performance battery-supercapacitor hybrid device

Measurement evidence

Microscopy Morphology

Self-assembled Mo doped Ni-MOF nanosheets based electrode material for high performance battery-supercapacitor hybrid device · Li Q., Guo H., Xue R. et al. · International Journal of Hydrogen Energy · 2020 · 20820-20831

2 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM and EDS elemental mapping/content distribution

Scanning electron microscopy Elemental microanalysis and mapping

M-NMN-1 · Electrode

SEM comparison of Ni-MOF and M-NMN-1/2/3; EDS mapping/content chart for M-NMN-1.

Temperature: about 298
Geometry: Powder/nanosheet material.
Context: Pristine Ni-MOF control and Mo-doped comparison series.
Measurement source: main p.4, article p.20823 · Results and discussion - Characterizations · Fig. 1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
M-NMN-1 actual Ni:Mo atom ratio	Ni:Mo = 1:1	—	—	Text Exact Reported	main p.3, article p.20822 · Results and discussion - Characterizations · Fig. 1j
M-NMN-1 EDS Mo content	Mo 10.70 wt%	—	wt% sigma 0.37	Figure Axis Rounded Reported	main p.4, article p.20823 · Results and discussion - Characterizations · Fig. 1j
M-NMN-1 EDS elemental wt% series	C 50.40 wt%; N 11.31 wt%; O 12.80 wt%; Ni 14.79 wt%; Mo 10.70 wt%	—	—	Figure Axis Rounded Reported	SI rendered p.4 · Supporting Information figures · Figure S1
M-NMN-1 morphologyMarked as a best value within this paper	large nanosheet structure formed by accumulation of small nanorods; looser pore structure and larger effective area	—	—	Text Qualitative	main p.3, article p.20822 · Results and discussion - Characterizations · Fig. 1c-d
Ni-MOF morphology	hexagonal short nanorod structure	—	—	Text Qualitative	main p.3, article p.20822 · Results and discussion - Characterizations · Fig. 1a-b

TEM, HR-TEM and SAED

Transmission electron microscopy

M-NMN-1 · Electrode

Detailed morphology and lattice imaging of M-NMN-1.

Temperature: about 298
Geometry: Nanosheet/nanorod material.
Context: Mo-doped target sample.
Measurement source: main p.3, article p.20822 · Results and discussion - Characterizations · Fig. 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
M-NMN-1 lattice fringe spacing	1.31 nm assigned to (001)	—	—	Text Exact Reported	main p.3, article p.20822 · Results and discussion - Characterizations · Fig. 2c-d
M-NMN-1 nanorod size in TEM	about 200-300 nm	—	—	Text Range	main p.3, article p.20822 · Results and discussion - Characterizations · Fig. 2a-b