Spectroscopy — Self-assembled Mo doped Ni-MOF nanosheets based electrode material for high performance battery-supercapacitor hybrid device

Measurement evidence

Spectroscopy

Self-assembled Mo doped Ni-MOF nanosheets based electrode material for high performance battery-supercapacitor hybrid device · Li Q., Guo H., Xue R. et al. · International Journal of Hydrogen Energy · 2020 · 20820-20831

4 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

M-NMN-2 EDS element distribution/content chart

M-NMN-2 · Electrode

EDS elemental composition chart in rendered SI Figure S1.

Temperature
about 298
Geometry
Powder/nanosheet material.
Context
Pristine Ni-MOF control and Mo-doped ratio series.
Measurement source
SI rendered p.4 · Supporting Information figures · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
M-NMN-2 EDS elemental wt% seriesC 53.36 wt%; N 8.96 wt%; O 18.85 wt%; Ni 8.28 wt%; Mo 10.54 wt%Figure Axis
Rounded Reported
SI rendered p.4 · Supporting Information figures · Figure S1

M-NMN-3 EDS element distribution/content chart

M-NMN-3 · Electrode

EDS elemental composition chart in rendered SI Figure S1.

Temperature
about 298
Geometry
Powder/nanosheet material.
Context
Pristine Ni-MOF control and Mo-doped ratio series.
Measurement source
SI rendered p.4 · Supporting Information figures · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
M-NMN-3 EDS elemental wt% seriesC 44.07 wt%; N 7.18 wt%; O 22.99 wt%; Ni 10.09 wt%; Mo 15.66 wt%Figure Axis
Rounded Reported
SI rendered p.4 · Supporting Information figures · Figure S1

Ni-MOF EDS element distribution/content chart

Ni-MOF · Electrode

EDS elemental composition chart in rendered SI Figure S1.

Temperature
about 298
Geometry
Powder/nanosheet material.
Context
Pristine Ni-MOF control and Mo-doped ratio series.
Measurement source
SI rendered p.4 · Supporting Information figures · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-MOF EDS elemental wt% seriesC 21.38 wt%; N 1.64 wt%; O 42.53 wt%; Ni 32.36 wt%Figure Axis
Rounded Reported
SI rendered p.4 · Supporting Information figures · Figure S1

X-ray photoelectron spectroscopy

M-NMN-1 · Electrode

Survey and high-resolution C 1s, Ni 2p, Mo 3d, N 1s and O 1s spectra of M-NMN-1.

Temperature
about 298
Geometry
Powder/nanosheet material.
Context
Mo-doped target sample.
Measurement source
main p.4, article p.20823 · Results and discussion - Characterizations · Fig. 4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
M-NMN-1 XPS survey elementsC, N, O, Ni and Mo coexistText
Qualitative
main p.4, article p.20823 · Results and discussion - Characterizations · Fig. 4a
Mo 3d Mo6+ binding energies232.0 eV (3d5/2) and 235.1 eV (3d3/2)Text
Exact Reported
main p.4, article p.20823 · Results and discussion - Characterizations · Fig. 4d
Ni 2p Ni3+/Ni2+ binding energiesNi3+ at 861.6 and 879.23 eV; Ni2+ at 855.6 and 873.3 eV; satellites at 864.8 and 882.2 eVText
Exact Reported
main p.4, article p.20823 · Results and discussion - Characterizations · Fig. 4c