Spectroscopy — Defect Engineering to Tailor Metal Vacancies in 2D Conductive Metal-Organic Frameworks: An Example in Electrochemical Sensing

Measurement evidence

Spectroscopy

Defect Engineering to Tailor Metal Vacancies in 2D Conductive Metal-Organic Frameworks: An Example in Electrochemical Sensing · Luo Y., Wu Y., Braun A. et al. · ACS Nano · 2022 · 20820-20830

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Raman spectroscopy and ATR-IR spectroscopy

Cu-BHT film prepared at pH 2 · Thin Film

Raman spectra for BHT and Cu-BHT pH series; ATR-IR spectra for BHT and Cu-BHT.

Geometry
thin films/powder reference
Context
pristine framework pH series
Measurement source
20823 · Results and Discussion · Figures S9-S10
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

High-resolution X-ray photoelectron spectroscopy (XPS), Al Kalpha radiation

Cu-BHT film prepared at pH 2 · Thin Film

Cu 2p and S 2p spectra for Cu-BHT pH series.

Geometry
thin films
Context
pristine framework pH series
Measurement source
20823-20824 · Results and Discussion · Figure 2b,c
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
S-Cu/S-C ratio pH 067:33Text
Rounded Reported
20824 · Results and Discussion · Figure 2c
S-Cu/S-C ratio pH 163:37Text
Rounded Reported
20824 · Results and Discussion · Figure 2c
S-Cu/S-C ratio pH 251:49Text
Rounded Reported
20824 · Results and Discussion · Figure 2c