Thermogravimetric analysis using PerkinElmer STA 6000
powder sample of compound 1 · Powder
N2 atmosphere; heating rate 10 C/min.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| no apparent weight loss up to temperature | up to 180 C | 453.15 K | — | Caption Exact Reported | p006 / SI p.S6 · Figure S4 caption · Figure S4 |
| first TGA mass-loss stage | 39.2% between 180 C and 270 C | 39.2 % | — | Caption Exact Reported | p006 / SI p.S6 · Figure S4 caption · Figure S4 |
| second TGA mass-loss stage | about 28.5% between 270 C and 460 C | 28.5 % | — | Caption Approximate | p006 / SI p.S6 · Figure S4 caption · Figure S4 |
| high-temperature TGA mass-loss stage | 27.5% beyond 500 C | 27.5 % | — | Caption Exact Reported | p006 / SI p.S6 · Figure S4 caption · Figure S4 |