Spectroscopy — Sulfur-Bridged Bonds Heightened Na-Storage Properties in MnS Nanocubes Encapsulated by S-Doped Carbon Matrix Synthesized via Solvent-Free Tactics for High-Performance Hybrid Sodium Ion Capacitors

Measurement evidence

Spectroscopy

Sulfur-Bridged Bonds Heightened Na-Storage Properties in MnS Nanocubes Encapsulated by S-Doped Carbon Matrix Synthesized via Solvent-Free Tactics for High-Performance Hybrid Sodium Ion Capacitors · Zhang H., Liu B., Lu Z. et al. · Small · 2023 · 2207214

3 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Raman spectroscopy

MSC-850 C-sublimed sulfur / MSC · Powder

Room-temperature Raman, excitation 488 nm; MC/MSC and temperature optimisation samples.

Temperature
room temperature
Geometry
powder
Context
derived composite and control
Measurement source
p004 · 2.1 Characterizations · Figure 2b; Figure S5
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
MC Raman ID/IGID/IG = 1.01Figure Axis
Rounded Reported
p004 · 2.1 Characterizations · Figure 2b
Mn-S/Mn-S-C Raman vibrationapproximately 654 cm-1approximatelyText
Approximate
p004 · 2.1 Characterizations · Figure 2b
MSC Raman ID/IGID/IG = 1.00Figure Axis
Rounded Reported
p004 · 2.1 Characterizations · Figure 2b

High-resolution XPS

MSC-850 C-sublimed sulfur / MSC · Powder

Mn 2p, S 2p and C 1s high-resolution spectra for MSC and MC comparison.

Geometry
powder
Context
MSC target and MC control
Measurement source
p004 · 2.1 Characterizations · Figure 2d-f
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
C-S-Mn/C-S C 1s binding energy285.5 eVText
Exact Reported
p005 · 2.1 Characterizations · Figure 2f
C-S-Mn Mn 2p XPS feature643.2 eVText
Exact Reported
p004 · 2.1 Characterizations · Figure 2d
MSC Mn 2p1/2 binding energy653.8 eVText
Exact Reported
p004 · 2.1 Characterizations · Figure 2d
MSC Mn 2p3/2 binding energy641.6 eVText
Exact Reported
p004 · 2.1 Characterizations · Figure 2d
C-S-Mn S 2p3/2 feature162.5 eVText
Exact Reported
p004 · 2.1 Characterizations · Figure 2e
C-S-Mn S 2p1/2 feature165.1 eVText
Exact Reported
p004 · 2.1 Characterizations · Figure 2e

FT-IR and X-ray photoelectron spectroscopy

Zn/Mn-MOFs · Powder

FT-IR spectra of Zn/MnCO3, H2BDC and Zn/Mn-MOFs; XPS survey and high-resolution C 1s spectra.

Geometry
powder
Context
MOF precursor characterisation
Measurement source
p003 · 2.1 Characterizations · Figure 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Zn/Mn-MOF C-O coordination XPS peakC-O peak at 285.3 eVText
Exact Reported
p003 · 2.1 Characterizations · Figure 1d