Powder X-ray diffraction (PXRD)
Complex 4 powder / pressed pellet · Powder
PXRD with Cu Kalpha radiation at room temperature; comparison among complexes 2, 3, 4, 7 and mixtures.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| PXRD distinct shifted peak, complex 4 | 2theta peak maximum 23.24 deg; higher than 2 (22.71), 3 (22.58), and mixture (22.69) | — | — | Text Rounded Reported | p004 · 3.3 Powder X-ray diffraction spectra · Fig. 2 |
| PXRD intense peak, complex 4 | distinct and more intense peak at 26.04 deg 2theta | — | — | Text Rounded Reported | p004 · 3.3 Powder X-ray diffraction spectra · Fig. 2 |
| PXRD broad symmetric peak, complex 4 | symmetrical peak from 26.83 to 29.21 deg 2theta, peak max 28.15 deg | — | — | Text Rounded Reported | p004-p005 · 3.3 Powder X-ray diffraction spectra · Fig. 2 |