Microscopy Morphology — Synthesis, characterization and solid state electrical properties of 1-D coordination polymer of the type [CuxNi1-x(dadb) ·yH2O]n

Measurement evidence

Microscopy Morphology

Synthesis, characterization and solid state electrical properties of 1-D coordination polymer of the type [CuxNi1-x(dadb) ·yH2O]n · Prasad R.L., Kushwaha A., Shrivastava O.N. · Journal of Solid State Chemistry · 2012 · 471-481

1 measurement group · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

TEM and electron diffraction

Complex 4 powder / pressed pellet · Powder

TEM on FEI Technai G2 F20 at 200 kV using copper grid for sample loading; representative complexes 2, 3 and 4.

Temperature
room temperature
Atmosphere
not specified
Geometry
powder on copper TEM grid
Context
pristine coordination polymer particles
Measurement source
p002 · 2.3 Analysis and physical measurements
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Average particle size, complex 2average particle size approx 40 nm; some approx 20 nm and some approx 103 nmText
Approximate
p008-p009 · 3.7 Transmission electron microscopy micrograph · Fig. 9
Average particle size, complex 3particle size approx 30 nmText
Approximate
p008-p009 · 3.7 Transmission electron microscopy micrograph · Fig. 9
Average particle size, complex 4average particle size approx 50 nmText
Approximate
p008-p009 · 3.7 Transmission electron microscopy micrograph · Fig. 9
Electron diffraction crystallinityregular pattern of spots in electron diffraction pattern of 2, 3 and 4 indicates microcrystalline nanoparticlesText
Qualitative
p008 · 3.7 Transmission electron microscopy micrograph · Fig. 9c