Three-dimensional electron diffraction, cRED, MicroED and related structure-solution methods.
Every source method stays verbatim. Subtypes retain distinctions such as ATR versus transmission IR, powder versus single-crystal diffraction, and two- versus four-contact transport.
The same technique may serve transport, electrochemistry, sensing or another scientific purpose.
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47 measurements
2025 · 2D Rhodium-Isocyanide Frameworks
as-prepared SJTU-201 powder · Powder · in-plane networks viewed along [001]; simulated TEM/ED compared with experiment
2025 · 2D Rhodium-Isocyanide Frameworks
as-prepared SJTU-202 powder · Powder · in-plane networks viewed along [001]; simulated TEM/ED compared with experiment
2025 · 2D Rhodium-Isocyanide Frameworks
as-prepared SJTU-203 powder · Powder · in-plane networks viewed along [001]; simulated TEM/ED compared with experiment
2025 · Asymmetrical Substitution Manipulates Stacking Modes in 2D Conductive MOF Crystals
Cu3F2HHTP2 blue powder/rod crystals · Powder · Synchrotron PXRD and cRED/SAED used to assign wavy bridged bilayer structure.
2025 · Asymmetrical Substitution Manipulates Stacking Modes in 2D Conductive MOF Crystals
Cu3FHHTP2 blue powder/rod crystals · Powder · Synchrotron PXRD and cRED/SAED used to assign layered structure and stacking.
2025 · Enhanced Electrical Conductivity by the Heavy Chalcogen Effect in Metal-Organic Frameworks
Cu-S-HHS solvothermal powder · Powder · Cu-S-HHS solved by MicroED at 77 K; Se/Te models Pawley-refined against PXRD.
2025 · Enhanced Electrical Conductivity by the Heavy Chalcogen Effect in Metal-Organic Frameworks
Cu-Se-HHS solvothermal powder · Powder · Cu-S-HHS solved by MicroED at 77 K; Se/Te models Pawley-refined against PXRD.
2025 · Enhanced Electrical Conductivity by the Heavy Chalcogen Effect in Metal-Organic Frameworks
Cu-Te-HHS solvothermal powder · Powder · Cu-S-HHS solved by MicroED at 77 K; Se/Te models Pawley-refined against PXRD.
2025 · High-resolution structure of Zn3(HOTP)2 (HOTP = hexaoxidotriphenylene), a three-dimensional conductive MOF
Zn3(HOTP)2 crystallites for 3D electron diffraction · Single Crystal · FEI Tecnai G2 20 TEM at 200 kV; Medipix 3 detector; tilt step 0.3 deg; 799 ms exposure per frame.
2025 · Volatolomics in Fritillarias and Their Identification by Orientation Controlled cMOF Thin Film Chemiresistors
Cu-HHTP[001]-20C thin film · Thin Film · TEM/SAED characterisation of Cu3(HHTP)2 film crystalline phase and lattice fringes.
2024 · Control of the Hydroquinone/Benzoquinone Redox State in High-Mobility Semiconducting Conjugated Coordination Polymers
Ag4TTBQ cRED TEM-grid nanocrystal sample · Single Crystal · TEM JEOL JEM2100 with LaB6 filament and ASI Timepix camera at 200 kV; REDp reconstruction, XRS intensity extraction, SHELXT structure solution.
2024 · Control of the Hydroquinone/Benzoquinone Redox State in High-Mobility Semiconducting Conjugated Coordination Polymers
Ag4TTHQ cRED TEM-grid nanocrystal sample · Single Crystal · TEM JEOL JEM2100 with LaB6 filament and ASI Timepix camera at 200 kV; REDp reconstruction, XRS intensity extraction, SHELXT structure solution.
2024 · De Novo Design and Facile Synthesis of Highly Crystalline 2D Conductive Metal-Organic Frameworks: A “Rotor-Stator” Strategy
Cu-DCB-MOF micrometer-sized crystal · Single Crystal · TEM JEM-F200, 200 kV; tilt range -44.9 to +62.2 deg; high vacuum below 1e-5 Pa; 298 K.
2024 · De Novo Design and Facile Synthesis of Highly Crystalline 2D Conductive Metal-Organic Frameworks: A “Rotor-Stator” Strategy
Cu-DCBBT-MOF black powder/crystals · Powder · TEM JEM-F200, 200 kV; tilt range -60.9 to +53.3 deg; high vacuum below 1e-5 Pa; 293 K.
2024 · De Novo Design and Facile Synthesis of Highly Crystalline 2D Conductive Metal-Organic Frameworks: A “Rotor-Stator” Strategy
Cu-DCBT-MOF black powder/crystals · Powder · TEM JEM-F200, 200 kV; tilt range -57.9 to +62.1 deg; high vacuum below 1e-5 Pa; 298 K.
2024 · Efficient oxygen evolution using conductive cobalt-based metal-organic framework
as-synthesised Co-BTB MOF powder · Powder · TEM/HRTEM imaging used to evaluate microstructure, lattice fringes, particle distribution, and crystallinity.
2024 · Gas-Induced Electrical and Magnetic Modulation of Two-Dimensional Conductive Metal–Organic Framework
NH3-exposed Cu3(C6O6)2 powder, 1% for 6 h · Powder · NH3-exposed powder; 200 kV electrons; TEM grid; cryo holder
2024 · Gas-Induced Electrical and Magnetic Modulation of Two-Dimensional Conductive Metal–Organic Framework
pristine Cu3(C6O6)2 powder · Powder · 200 kV electrons; TEM grid; cryo holder; 293 K table value
2024 · Synthesis and structure of a non-van-der-Waals two-dimensional coordination polymer with superconductivity
Pulverised Cu3BHT powder for Micro-ED · Powder · JEOL JEM2100 TEM at 200 kV with Timepix detector; specimen cooled to 96 K; goniometer rotation; 0.5 s exposures.
2023 · Ligand-Oxidation-Based Anodic Synthesis of Oriented Films of Conductive M-Catecholate Metal-Organic Frameworks with Controllable Thickness
Cu3(HHTP)2 film on Au/Cr/glass anode deposited at 0.25 V for 45 min · Thin Film · Fragment removed from Au electrode and settled on TEM grid with (002) plane parallel to electron beam.
2023 · Near IR Bandgap Semiconducting 2D Conjugated Metal-Organic Framework with Rhombic Lattice and High Mobility
Cu2(OHPTP) rod-like single crystals · Single Crystal · cRED on JEOL JEM2100 using Instamatic; ED processed with XDS, solved with Shelx-2017 and refined with Shelxl-2017; Pawley refinement in TOPAS Academic V4.1.
2023 · Self-Powered Infrared Photodetectors with Ultra-High Speed and Detectivity Based on Amorphous Cu-Based MOF Films
p-a-Cu-HHTP MOF film on electrospun nanofibres · Thin Film · Phase/crystallinity assessment of p-a-Cu-HHTP MOF film.
2023 · Semiconducting Conjugated Coordination Polymer with High Charge Mobility Enabled by “4 + 2” Phenyl Ligands
as-synthesised Cu4DHTTB crystals/powder · Powder · 3D ED data collected on JEOL JEM2100 TEM at 200 kV; PXRD with Cu K alpha radiation over 5-80 deg 2theta in Bragg-Brentano reflection mode.
2023 · Wavy Two-Dimensional Conjugated Metal-Organic Framework with Metallic Charge Transport
Isolated Cu3(HFcHBC)2 single crystal device · Single Crystal · Single crystal dispersed in ethanol, transferred to holey carbon copper grid; JEOL JEM2100 at 200 kV; tilt rate 0.45 deg s-1 and exposure 0.5 s per frame.
2022 · A Monocrystalline Coordination Polymer with Multiple Redox Centers as a High-Performance Cathode for Lithium-Ion Batteries
as-synthesised CuCA nanosheet powder · Nanosheet · Morphology, nanosheet dimensions, monocrystalline nature, and elemental distribution for as-synthesised CuCA.
2022 · Adjustable Synthesis of Ni-Based Metal-Organic Framework Membranes and Their Field-Effect Transistor Sensors for Mercury Detection
S4 Ni3(HITP)2 membrane · Thin Film · Nanostructure/crystallinity and elemental distribution of S4 sample.
2022 · Chemical Vapor Deposition of Edge-on Oriented 2D Conductive Metal-Organic Framework Thin Films
Scraped Cu3(C6O6)2 powder pellet · Pellet · Scraped thin-film product transferred to TEM grid; HRTEM zone-axis and FFT analysis.
2022 · Conductive Hybrid Cu-HHTP-TCNQ Metal–Organic Frameworks for Chemiresistive Sensing
Cu-HHTP-TCNQ film on copper TEM grid, 40 min · Thin Film · JEOL 2200FS, 200 keV, 0.3 s exposure; SAED camera lengths 100 and 60 cm.
2022 · Dimensionality Modulates Electrical Conductivity in Compositionally Constant One-, Two-, and Three-Dimensional Frameworks
Fresh Ni-2D rods · Powder · Crystals dispersed in ethanol, cooled to 96 K, JEOL JEM-2100 at 200 kV; five datasets merged.
2022 · Dimensionality Modulates Electrical Conductivity in Compositionally Constant One-, Two-, and Three-Dimensional Frameworks
Ni-3D-ox from ambient workup · Powder · Four cRED datasets collected on individual crystals; hexagonal indexing; PLATON/SQUEEZE used for disordered guest contribution.
2022 · Microscopic Insights into Cation-Coupled Electron Hopping Transport in a Metal-Organic Framework
bulk Zr(dcphOH-NDI) crystals for 3DED · Single Crystal · Bulk Zr(dcphOH-NDI) crystals measured by continuous-rotation electron diffraction at cryogenic temperature.
2022 · sp-Carbon Incorporated Conductive Metal-Organic Framework as Photocathode for Photoelectrochemical Hydrogen Generation
Cu3HHAE2 single crystals for cRED · Single Crystal · cRED collected at 96 K with Timepix detector in video mode; processed by REDp/XDS, solved with SHELXT, refined against PXRD with Topas 6.1.
2021 · Conductive Stimuli-Responsive Coordination Network Linked with Bismuth for Chemiresistive Gas Sensing
Bi(HHTP)-alpha MicroED crystal · Single Crystal · Thermo Fisher Talos F200C/CetaD; 200 keV; CIF data_merge_a
2021 · Conductive Stimuli-Responsive Coordination Network Linked with Bismuth for Chemiresistive Gas Sensing
Bi(HHTP)-beta hydrated MicroED crystal · Single Crystal · CIF data_mov01_a; hydrated/water-containing beta form
2021 · Conductive Stimuli-Responsive Coordination Network Linked with Bismuth for Chemiresistive Gas Sensing
NH3-exposed Bi(HHTP) · Powder · Bi(HHTP) exposed to 10,000 ppm NH3 for 1 h; CIF BiHHTP_NH3
2021 · Conductive Stimuli-Responsive Coordination Network Linked with Bismuth for Chemiresistive Gas Sensing
NO-exposed Bi(HHTP) · Powder · Bi(HHTP) exposed to 10,000 ppm NO for 1 h; CIF BiHHTP_NO
2021 · Conductive Stimuli-Responsive Coordination Network Linked with Bismuth for Chemiresistive Gas Sensing
Bi(HHTP)-alpha MicroED crystal · Single Crystal · BIOVIA Materials Studio Pawley refinement of activated Bi(HHTP)
2020 · Conjugated Copper–Catecholate Framework Electrodes for Efficient Energy Storage
As-synthesised Cu-DBC powder · Powder · Single submicrometre Cu-DBC crystals; specimen plus electron-beam tilt from -50 to +50 degrees with 0.3 degree beam-tilt step; HRTEM at 200 kV.
2020 · Metal-organic framework nanosheets for enhanced performance of organic photovoltaic cells
Zn2(ZnTCPP) MON suspension · Nanosheet · AFM on mica; TEM on holey C-coated Cu grid after dropcasting 10 uL suspension; JEOL-2010F at 200 kV.
2020 · Paramagnetic Conducting Metal–Organic Frameworks with Three-Dimensional Structure
Co-THBQ well-crystallised powder · Powder · Themis 300 TEM, 300 kV, lambda 0.01971 A; sample cooled to 94 K; -45 to 50 deg range with 1 deg step; 2 s exposure; 96 frames; solved/refined with Olex2.
2019 · Electrocatalytic Hydrogen Evolution from a Cobaloxime-Based Metal-Organic Framework Thin Film
Bulk UU-100(Co) powder · Powder · cRED under cryogenic conditions; PXRD Cu K-alpha; structural model refined with DFT.
2018 · High-mobility band-like charge transport in a semiconducting two-dimensional metal–organic framework
Large-area free-standing Fe3(THT)2(NH4)3 multilayer film · Thin Film · Structural and morphological characterisation of free-standing/transferred films at room temperature.
2018 · Highly Conducting Neutral Coordination Polymer with Infinite Two-Dimensional Silver-Sulfur Networks
Ag-BHT nanocrystals exfoliated from film · Unknown · PXRD collected with Cu Kalpha radiation, 40 kV and 40 mA, 2theta 5.0-120.0 degrees, 0.013 degree step, 406 s per step; RED used for 3D reciprocal lattice reconstruction.
2017 · Colossal Increase in Electric Current and High Rectification Ratio in a Photoconducting, Self-Cleaning, and Luminescent Schottky Barrier NMOF Diode
NMOF-1 bulk nanosheets/powder · Nanosheet · FESEM on silicon wafer; TEM after ethanol sonication/drop-casting on carbon-coated Cu grid; AFM height profiles
2017 · Conductive Metal–Organic Framework Nanowire Array Electrodes for High-Performance Solid-State Supercapacitors
Cu-CAT nanowire arrays on carbon fibre paper · Electrode · TEM at 200 kV; lattice fringes and SAED used to assign single-crystal character and [001] growth direction.
2012 · Synthesis, characterization and solid state electrical properties of 1-D coordination polymer of the type [CuxNi1-x(dadb) ·yH2O]n
Complex 4 powder / pressed pellet · Powder · TEM on FEI Technai G2 F20 at 200 kV using copper grid for sample loading; representative complexes 2, 3 and 4.
2010 · Highly conducting two-dimensional copper(i) 4-hydroxythiophenolate network
polycrystalline CuHT yellow powder · Powder · FEI Philips Tecnai 20 TEM; individual platy crystallite viewed along [100].
No mapped measurement matches these filters.
These are the exact source-preserving method strings consolidated by this technique group.
| Raw method label | Mapped measurements |
|---|---|
| 3D electron diffraction; ab initio solution and SHELXL refinement | 3 |
| PXRD and MicroED/Pawley structural analysis | 3 |
| AC-HRTEM and electron diffraction | 3 |
| MicroED crystal-structure solution | 2 |
| PXRD and cRED | 2 |
| Continuous rotation electron diffraction (cRED) | 2 |
| TEM and electron diffraction | 2 |
| MicroED | 2 |
| Cross-section SEM, TEM, HRTEM, selected-area electron diffraction and PXRD with DFT comparison | 1 |
| TEM and selected-area electron diffraction | 1 |
| MicroED after NH3 exposure | 1 |
| MicroED after NO exposure | 1 |
| Pawley refinement of pXRD using MicroED CIF | 1 |
| 3D electron diffraction tomography, HRTEM, SAED | 1 |
| continuous rotation electron diffraction (cRED) | 1 |
| Microcrystal electron diffraction (Micro-ED) in TEM | 1 |
| Transmission electron microscopy (TEM) and selected area electron diffraction (SAED) | 1 |
| TEM/HRTEM/FFT/electron diffraction | 1 |
| Continuous-rotation electron diffraction and Pawley refinement | 1 |
| Three-dimensional electron diffraction / selected-area electron diffraction | 1 |
| continuous rotation electron diffraction (c-RED), PXRD Pawley/Rietveld refinement | 1 |
| FESEM, TEM, HRTEM, electron diffraction and AFM | 1 |
| cRED / MicroED and PXRD Pawley fitting | 1 |
| 3D electron diffraction / MicroED; PETS2, Jana2020, Superflip refinement in superspace | 1 |
| Continuous rotation electron diffraction (cRED), SHELXT/SHELXL refinement | 1 |
| cRED structure solution and refinement | 1 |
| three-dimensional electron diffraction (3DED) | 1 |
| HRTEM, selected-area electron diffraction and EDS mapping | 1 |
| SEM, TEM, selected area electron diffraction, elemental mapping | 1 |
| AFM, TEM, HR-TEM, FFT electron diffraction and EELS | 1 |
| TEM and selected area electron diffraction (SAED) | 1 |
| rotation electron diffraction plus powder X-ray diffraction Rietveld refinement | 1 |
| TEM, HR-TEM and selected-area electron diffraction | 1 |
| continuous rotation electron diffraction (cRED) and structure solution | 1 |
| XRD and selected-area electron diffraction (SAED) | 1 |
| HRTEM and selected-area electron diffraction (SAED) | 1 |