HRTEM and selected-area electron diffraction (SAED)
as-synthesised Co-BTB MOF powder · Powder
TEM/HRTEM imaging used to evaluate microstructure, lattice fringes, particle distribution, and crystallinity.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| lattice spacing annotation | 0.24 nm | 0.24 nm | figure annotation | Visual Estimate Approximate | 4 · Figure · Figure 5e |
| average interlayer spacing from text | ~0.2 nm | 0.2 nm | ~ | Text Approximate | 5 · Result and discussion · Figure 5e |
| TEM particle distribution | evenly distributed, devoid of aggregation or clustering | — | — | Text Qualitative | 5 · Result and discussion · Figure 5c,d |
| SAED crystallinity | distinct diffraction spots indicating regular atomic arrangement | — | — | Text Qualitative | 5 · Result and discussion · Figure 5f |