Diffraction Structure — Efficient oxygen evolution using conductive cobalt-based metal-organic framework

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction (PXRD)

X-ray diffraction and scattering

cobalt oxide control powder · Powder

Cobalt oxide control PXRD shown in Figure S1a; SI methods report Rigaku MiniFlex with Cu-Kalpha radiation, 2theta range 5-30 deg, though the rendered panel spans approximately 30-60 deg.

Context: non-MOF cobalt oxide control powder
Measurement source: 5 · Figure S1 · Figure S1a

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Co3O4 control PXRD phase assignment	PXRD pattern assigned to Co3O4 / JCPDS 00-042-1467	—	—	Figure Axis Qualitative	5 · Figure S1 · Figure S1a

Powder X-ray diffraction (PXRD)

X-ray diffraction and scattering

as-synthesised Co-BTB MOF powder · Powder

Rigaku MiniFlex with Cu-Kalpha radiation; data acquired over 2theta = 5-30 deg; synthesised Co-BTB compared with simulated Co-MOF.

Context: pristine framework powder
Measurement source: SI text · Materials and General Methods

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Co-BTB PXRD characteristic peak, (0 1 1)	2theta = 5.67 deg (0 1 1)	—	—	Text Exact Reported	2 · Result and discussion · Figure 2a
Co-BTB PXRD characteristic peak, (1 2 1)	2theta = 10.02 deg (1 2 1)	—	—	Text Exact Reported	2 · Result and discussion · Figure 2a