Diffraction Structure — Highly Conducting Neutral Coordination Polymer with Infinite Two-Dimensional Silver-Sulfur Networks

Measurement evidence

Diffraction Structure

Highly Conducting Neutral Coordination Polymer with Infinite Two-Dimensional Silver-Sulfur Networks · Huang X., Li H., Tu Z. et al. · Journal of the American Chemical Society · 2018 · 15153-15156

1 measurement group · 13 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

rotation electron diffraction plus powder X-ray diffraction Rietveld refinement

X-ray diffraction and scattering Electron diffraction

Ag-BHT nanocrystals exfoliated from film · Unknown

PXRD collected with Cu Kalpha radiation, 40 kV and 40 mA, 2theta 5.0-120.0 degrees, 0.013 degree step, 406 s per step; RED used for 3D reciprocal lattice reconstruction.

Context: pristine Ag-BHT structure determination
Measurement source: S5, S20 · X-ray diffraction characterization and analysis · Figure 2; Figure S4; Table S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ag-Ag bond length	2.88 A	—	—	Text Exact Reported	p002 / 15154 · Results and discussion · Figure S6
Ag-Ag bond length	3.03 A	—	—	Text Exact Reported	p002 / 15154 · Results and discussion · Figure S6
Ag-Ag bond length	3.13 A	—	—	Text Exact Reported	p002 / 15154 · Results and discussion · Figure S6
unit-cell a	15.1168(19) A	—	(19)	SI Table Exact Reported	S20 · Table S1 · Table S1
unit-cell b	9.1042(13) A	—	(13)	SI Table Exact Reported	S20 · Table S1 · Table S1
unit-cell beta angle	110.430(3) degrees	—	(3)	SI Table Exact Reported	S20 · Table S1 · Table S1
unit-cell c	4.2776(6) A	—	(6)	SI Table Exact Reported	S20 · Table S1 · Table S1
unit-cell volume	551.67(13) A^3	—	(13)	SI Table Exact Reported	S20 · Table S1 · Table S1
refined chemical formula	Ag5C6S6	—	—	SI Table Exact Reported	S20 · Table S1 · Table S1
interlayer distance of 2D networks	7.0 A	—	—	Text Rounded Reported	p002 / 15154 · Results and discussion · Figure 3
Rietveld Rp	3.45%	—	—	SI Table Exact Reported	S20 · Table S1 · Table S1
Rietveld Rwp	4.98%	—	—	SI Table Exact Reported	S20 · Table S1 · Table S1
space group	I2/m	—	—	SI Table Exact Reported	S20 · Table S1 · Table S1