Diffraction Structure — High-mobility band-like charge transport in a semiconducting two-dimensional metal–organic framework

Measurement evidence

Diffraction Structure

High-mobility band-like charge transport in a semiconducting two-dimensional metal–organic framework · Dong R., Han P., Arora H. et al. · Nature Materials · 2018 · 1027-1032

1 measurement group · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Cross-section SEM, TEM, HRTEM, selected-area electron diffraction and PXRD with DFT comparison

X-ray diffraction and scattering Electron diffraction Scanning electron microscopy Transmission electron microscopy Density functional theory

Large-area free-standing Fe3(THT)2(NH4)3 multilayer film · Thin Film

Structural and morphological characterisation of free-standing/transferred films at room temperature.

Temperature: about 300
Geometry: Multilayer film.
Context: pristine framework
Measurement source: main p.2, article p.1028 · Synthesis and sample characterization · Fig. 1; Supplementary Figs. S1-S3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Film thickness after 72 h reaction	~2 um for 72 reaction hours	—	—	Text Approximate	main p.2, article p.1028 · Synthesis and sample characterization · Fig. 1a
Hall-bar film thickness	1.7 +/- 0.1 um	—	+/- 0.1 um	Caption Exact Reported	SI p.5/44 · Structural characterization · Fig. S1
Interlayer distance	~0.33 nm	—	—	Text Approximate	main p.2, article p.1028 · Synthesis and sample characterization · Fig. 1c
Honeycomb pore size	~1.9 nm	—	—	Text Approximate	main p.2, article p.1028 · Synthesis and sample characterization · Fig. 1b; Fig. S2c
PXRD (001) stacking peak position	2theta = 27.3 deg	—	—	Text Rounded Reported	main p.2, article p.1028 · Synthesis and sample characterization · Fig. 1c
PXRD (100) peak position	2theta = 4.5 deg	—	—	Text Rounded Reported	main p.2, article p.1028 · Synthesis and sample characterization · Fig. 1c
PXRD (200) peak position	2theta = 9.1 deg	—	—	Text Rounded Reported	main p.2, article p.1028 · Synthesis and sample characterization · Fig. 1c
In-plane unit-cell dimension from SAED	~1.97 nm	—	—	Caption Approximate	SI p.6/44 · Structural characterization · Fig. S2