Diffraction Structure — Conjugated Copper–Catecholate Framework Electrodes for Efficient Energy Storage

3 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

As-synthesised Cu-DBC powder · Powder

Single submicrometre Cu-DBC crystals; specimen plus electron-beam tilt from -50 to +50 degrees with 0.3 degree beam-tilt step; HRTEM at 200 kV.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
3D-EDT reconstructed a parameter	a = 34.8 angstrom	—	—	Text Rounded Reported	S6 · Section 6. 3D-EDT Measurement · Figure S4
3D-EDT reconstructed b parameter	b = 42.7 angstrom	—	—	Text Rounded Reported	S6 · Section 6. 3D-EDT Measurement · Figure S4
3D-EDT reconstructed c parameter	c = 14.9 angstrom	—	—	Text Rounded Reported	S6 · Section 6. 3D-EDT Measurement · Figure S4
Rhombic pore spacing d020	d020 = 21.16 angstrom	—	—	Text Exact Reported	1082 · Results and discussion · Figure 1f,g; Figure S6
Rhombic pore spacing d200	d200 = 16.95 angstrom	—	—	Text Exact Reported	1082 · Results and discussion · Figure 1f,g; Figure S6

As-synthesised Cu-DBC powder · Powder

RIGAKU SMARTLAB9KW, Cu target tube and K beta filter; Pawley refinement against PXRD.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Pawley refined a parameter	a = 34.4 angstrom	—	—	Text Rounded Reported	1082 · Results and discussion · Figure 1b
Pawley refined b parameter	b = 42.6 angstrom	—	—	Text Rounded Reported	1082 · Results and discussion · Figure 1b
Pawley refined c parameter	c = 14.6 angstrom	—	—	Text Rounded Reported	1082 · Results and discussion · Figure 1b
Pawley refined unit cell volume	V = 21395 angstrom3	—	—	Text Rounded Reported	1082 · Results and discussion · Figure 1b
Possible space group	P212121 (No. 19)	—	—	Text Qualitative	1082 · Results and discussion · Figure 1b

As-synthesised Cu-DBC powder · Powder

Cu-DBC immersed in nine solvents for seven days; SEM after water immersion.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Solvent stability by PXRD	No obvious PXRD change after immersion in nine different solvents for seven days.	—	—	Text Qualitative	1083 · Results and discussion · Figure S17