Diffraction Structure — Synthesis and structure of a non-van-der-Waals two-dimensional coordination polymer with superconductivity

2 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Pulverised Cu3BHT powder for Micro-ED · Powder

JEOL JEM2100 TEM at 200 kV with Timepix detector; specimen cooled to 96 K; goniometer rotation; 0.5 s exposures.

Temperature: 96
Atmosphere: TEM vacuum
Context: pristine Cu3BHT microcrystal
Measurement source: 2 · Single crystal structure characterization of Cu3BHT · Figure 1f

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Interlayer Cu-S covalent contactMarked as a best value within this paper	2.662(6) Angstrom	—	(6)	Text Exact Reported	3 · Single crystal structure characterization of Cu3BHT · Figure 1b,c
Cu-S coordination bond distance range	2.26(1) to 2.33(9) Angstrom	—	range with reported uncertainties	Text Range	2 · Single crystal structure characterization of Cu3BHT · Supplementary Fig. 10
Average interlayer distance	3.32 Angstrom	—	—	Text Rounded Reported	3 · Single crystal structure characterization of Cu3BHT · Figure 1b
Micro-ED unit-cell volume	870.6(3) Angstrom3	—	(3)	Table Exact Reported	29 · Supplementary Table 1 · Supplementary Table 1
Micro-ED resolutionMarked as a best value within this paper	0.696 Angstrom	—	—	Text Exact Reported	2 · Single crystal structure characterization of Cu3BHT · Figure 1f

Cu3BHT micro-crystal array / multicrystalline film · Thin Film

Synchrotron radiation lambda = 0.458086 Angstrom; lab PXRD Cu Kalpha lambda = 1.5406 Angstrom, 2theta 5-60 degrees, 0.023 degree step, 60 s exposure.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Unit-cell a parameter	a = 14.8082(10) Angstrom	—	(10)	Text Exact Reported	2 · Synthesis of Cu3BHT micro-crystal array · Figure 1g
Unit-cell b parameter	b = 8.6706(6) Angstrom	—	(6)	Text Exact Reported	2 · Synthesis of Cu3BHT micro-crystal array · Figure 1g
Unit-cell beta angle	beta = 97.342(2) degrees	—	(2)	Text Exact Reported	2 · Synthesis of Cu3BHT micro-crystal array · Figure 1g
Unit-cell c parameter	c = 6.8357(5) Angstrom	—	(5)	Text Exact Reported	2 · Synthesis of Cu3BHT micro-crystal array · Figure 1g
Resolved low-angle PXRD peaks	3.51 and 3.57 degrees; d-spacing = 7.4788 and 7.3531 Angstrom; indexed as (110) and (200)	—	—	Text Exact Reported	2 · Synthesis of Cu3BHT micro-crystal array · Figure 1g
Refined space groupMarked as a best value within this paper	P21/c	—	—	Text Exact Reported	2 · Single crystal structure characterization of Cu3BHT · Figure 1