Thermogravimetric analysis
air-stabilised Fe2(DHBQ)3 powder · Powder
TG under nitrogen and air at 10 C min-1.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Decomposition temperature in air | about 200 C in air | — | — | Text Approximate | 428 · 2.1 · Fig. 1f |
| Decomposition temperature in nitrogen | about 350 C in nitrogen | — | — | Text Approximate | 428 · 2.1 · Fig. 1f |
| Fe content by ICP-OES | 20.0 wt% | — | — | Text Exact Reported | 428 · 2.1 |
| Fe content calculated from TG/Fe2O3 residue | 19.4 wt% Fe | — | — | Calculated From Reported Rounded Reported | 428 · 2.1 · Fig. 1f, Fig. S4 |
| Fe content in proposed formula | Fe content 19.9 wt% in Fe2(C6H2O4)3.2H2O | — | — | Calculated From Reported Rounded Reported | 428 · 2.1 |
| Water content in proposed formula | H2O content 6.4 wt% in Fe2(C6H2O4)3.2H2O | — | — | Calculated From Reported Rounded Reported | 428 · 2.1 |
| Residual weight at 600 C after calcination | 27.7% at 600 C | — | — | Text Exact Reported | 428 · 2.1 · Fig. 1f, Fig. S4 |
| Minor mass loss assigned to absorbed water | approximately 6.8% in air before the major loss | — | — | Text Approximate | 428 · 2.1 · Fig. 1f |