Other — Novel semiconducting iron–quinizarin metal–organic framework for application in supercapacitors*

Measurement evidence

Other

Novel semiconducting iron–quinizarin metal–organic framework for application in supercapacitors* · Agrawal S., Clarke S.M., Vitorica-Yrezabal I.J. et al. · Molecular Physics · 2019 · 3424-3433

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Elemental analysis; CHN by combustion and metals by ICP-OES as described generally

as-synthesised FeQ black precipitate / powder with small crystals · Powder

Product composition compared with calculated Fe(C14H6O4).H2O formula

Context
pristine framework powder
Measurement source
p007 · 3. FeQ synthesis
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
measured C contentC-53.58 wt%; calculated C-53.88 wt%Text
Exact Reported
p007 · 3. FeQ synthesis
measured Fe contentFe-17.22 wt%; calculated Fe-17.89 wt% for Fe(C14H6O4).H2OText
Exact Reported
p007 · 3. FeQ synthesis
measured H contentH-3.20 wt%; calculated H-2.58 wt%Text
Exact Reported
p007 · 3. FeQ synthesis

Thermogravimetric analysis (TGA Q 500)

as-synthesised FeQ black precipitate / powder with small crystals · Powder

Heating rate 10 deg C min^-1 under inert nitrogen atmosphere

Atmosphere
nitrogen
Geometry
powder sample
Context
pristine framework powder
Measurement source
p007 · 2.3. Characterisation of materials
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
quinizarin ligand decomposition comparisonligand-quinizarin decomposes at approximately 180 deg CapproximatelyCaption
Approximate
p009 · Figure 3 caption · Figure 3
thermal stability onset / mass reduction temperatureFeQ mass reduction at approximately 270 deg C; stable up to 270 deg CapproximatelyText
Approximate
p008-p009 · 4. Results · Figure 3