Other — One‐Pot hydrothermal synthesis of 1D copper (II) coordination polymers involving in-situ decarboxylation

2 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

CP 1 dark blue crystals · Single Crystal

50-1100 C under N2 at 10 C min^-1.

Atmosphere: N2
Context: pristine framework crystal
Measurement source: main p.6 · 3.5. Thermal properties and PXRD patterns · Figures S6-S7

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
CP 1 organic ligand decomposition mass loss	71.33% in 280-350 C	—	—	Text Exact Reported	main p.6 · 3.5. Thermal properties and PXRD patterns · Figure S6
CP 1 first TGA mass loss	5.76% in 83-125 C	—	—	Text Exact Reported	main p.6 · 3.5. Thermal properties and PXRD patterns · Figure S6
CP 1 thermal stability upper temperatureMarked as a best value within this paper	thermally stable up to 280 C	—	—	Text Exact Reported	main p.6 · 3.5. Thermal properties and PXRD patterns · Figure S6

CP 2 green crystals · Single Crystal

50-1100 C under N2 at 10 C min^-1.

Atmosphere: N2
Context: pristine framework crystal
Measurement source: main p.6 · 3.5. Thermal properties and PXRD patterns · Figures S6-S7

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
CP 2 phenanthroline-ligand decomposition mass loss	46.78%	—	—	Text Exact Reported	main p.6 · 3.5. Thermal properties and PXRD patterns · Figure S7
CP 2 sulfate-ligand decomposition mass loss	23.50% in 217-440 C	—	—	Text Exact Reported	main p.6 · 3.5. Thermal properties and PXRD patterns · Figure S7
CP 2 first TGA mass loss	9.98% in 110-218 C	—	—	Text Exact Reported	main p.6 · 3.5. Thermal properties and PXRD patterns · Figure S7