Measurement evidence
Oxidatively Doped Tetrathiafulvalene-Based Metal-Organic Frameworks for High Specific Energy of Supercapatteries · Ren Z.-H., Zhang Z.-R., Ma L.-J. et al. · ACS Applied Materials and Interfaces · 2023 · 6621-6630
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
1 crystals · Single Crystal
Weight loss before 300 degC attributed to loss of two cocrystallized water molecules.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TGA weight loss before 300 degC | 5.25% | — | — | Text Exact Reported | p003 / 6623 · 2.2 · Figure 2a |
1-ox' · Powder
Iodine release after cocrystallized water loss in washed 1-ox' sample.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| mass increase after iodine vapour treatment | ca. 24% increase in mass for 1-ox | — | ca. | Text Approximate | p008 / 6628 · 4.1.3 Iodine-Treated 1 (1-ox) |
| iodine-release weight loss | 4.1% | — | — | Text Exact Reported | p003 / 6623 · 2.2 · Figure 2a |
| iodine-to-py-TTF-py ratio in 1-ox and 2-ox from EA | I amount is 1.32 times that of py-TTF-py | — | — | Text Exact Reported | p003 / 6623 · 2.2 |
| fraction of TTF moieties oxidised after iodine treatment | only a few TTF moieties (12%) ... become radical cations | — | — | Text Exact Reported | p003 / 6623 · 2.2 · Figure S3 referenced |
2 crystals · Single Crystal
Weight loss before 300 degC attributed to loss of two cocrystallized water molecules.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TGA weight loss before 300 degC | 5.15% | — | — | Text Exact Reported | p003 / 6623 · 2.2 · Figure S3 referenced |