Diffraction Structure — Efficient hydrogen production from MIL-53(Fe) catalyst-modified Mo: BiVO4 photoelectrodes

2 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FMBV-2 / 2% Mo:BiVO4-MIL-53(Fe) · Electrode

FMBV-2 and pure 2% Mo:BiVO4 compared; XPS elemental spectra for FMBV.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
FMBV XPS elemental composition	Fe, C, O, Mo, Bi and V present	—	—	Text Qualitative	4 · Results and discussion · Fig. S4
FMBV XRD phase assignment	characteristic peaks indexed to monoclinic BiVO4; no additional MIL-53(Fe) peaks observed	—	—	Text Qualitative	4 · Results and discussion · Fig. 3A; Fig. S3

as-prepared MIL-53(Fe) powder · Powder

Cu Kalpha radiation, 40 kV and 40 mA.

Geometry: powder
Context: pristine MIL-53(Fe) component
Measurement source: 2-3 · Materials and instruments; Results and discussion · Fig. 1C-D

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
MIL-53(Fe) framework and pore dimensionality	three-dimensional framework with a one-dimensional pore channel system	—	—	Text Qualitative	3 · Results and discussion · Fig. 1D
MIL-53(Fe) phase assignment	monoclinic symmetry, matching crystalline MIL-53(Fe) framework	—	—	Text Qualitative	3 · Results and discussion · Fig. 1C