Measurement evidence
Cluster-Bridging-Coordinated Bimetallic Metal−Organic Framework as High-Performance Anode Material for Lithium-Ion Storage · Yan W., Fan K., Zheng L.-M. et al. · Small Structures · 2021 · 2100122
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
As-synthesised Co4-Ir MOF crystal/powder · Powder
Bruker D8 ADVANCE with Cu Kalpha radiation; HCl-amount optimisation shown from 10 to 60 uL in SI Figure S1.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| optimal HCl amount | 23 uL HCl | — | — | Text Exact Reported | 2 · Results and Discussion · Figure S1 |
| PXRD pattern match | as-measured PXRD pattern identical to simulated pattern | — | — | Text Qualitative | 2 · Results and Discussion · Figure 1e |
As-synthesised Co4-Ir MOF crystal/powder · Powder
Crystallographic data reported in SI Table S1; selected bond lengths and angles in Table S2.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| CCDC number | 2078073 | — | — | SI Table Exact Reported | 2 · Table S1 · Table S1 |
| Co-Ocarboxylate bond length range | 2.066-2.189 A | — | — | Text Range | 2 · Results and Discussion · Table S2 |
| Co-Ocenter bond lengths | 1.851 and 1.973 A | — | — | Text Rounded Reported | 2 · Results and Discussion · Table S2 |
| crystalline system | trigonal | — | — | SI Table Exact Reported | 2 · Table S1 · Table S1 |
| framework formula in crystallographic table | C72H42Co4Ir2N6O13 | — | — | SI Table Exact Reported | 2 · Table S1 · Table S1 |
| closest interlayer distance | 3.6 A | — | — | Text Rounded Reported | 2 · Results and Discussion |
| open channel size | 5.8 x 3.6 A | — | — | Text Rounded Reported | 2 · Results and Discussion |
| space group | R-3 | — | — | SI Table Exact Reported | 2 · Table S1 · Table S1 |
| unit cell a | 14.185(3) A | — | (3) | SI Table Exact Reported | 2 · Table S1 · Table S1 |
| unit cell c | 38.969(9) A | — | (9) | SI Table Exact Reported | 2 · Table S1 · Table S1 |
| unit cell volume | 6791(4) A3 | — | (4) | SI Table Exact Reported | 2 · Table S1 · Table S1 |