Diffraction Structure — Electrocatalytic oxygen evolution reaction at IrOx supported by Ni/Co-ZIF-67: Controlled ratio of metallic Ir and Ir3+ states

3 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

2.8-IrOx@Ni/Co-ZIF-67 / IrOx@Ni/Co-ZIF-67 · Nanosheet

XRD of Ni/Co-ZIF-67 and IrOx@Ni/Co-ZIF-67 with different IrOx contents.

Context: target composite
Measurement source: article p4 · Results and discussion · Figure 2a; Figure S7

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
IrOx crystalline XRD peaks	IrOx peaks could not be detected; Ni/Co-ZIF-67 characteristic peaks retained with decreasing intensity at higher IrOx loading	—	—	Text Qualitative	article p4 · Results and discussion · Figure 2a; Figure S7

Ni/Co-ZIF-67-2 / Ni/Co-ZIF-67 · Nanosheet

Same powder XRD method; comparison with standard ZIF-67 and pristine ZIF-67.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Secondary phase detection	No peaks relating to other secondary phases were detected	—	—	Text Qualitative	article p3 · Results and discussion · Figure 1a; Figure S1

ZIF-67 nanosheet powder/control · Nanosheet

X'Pert PRO, Cu Kalpha radiation, 40 kV/30 mA, 2theta 10-80 deg, scan speed 0.02 deg s^-1.

Geometry: powder XRD
Context: pristine ZIF-67 control
Measurement source: article p2-p3 · Material characterizations / Results · Figure 1a

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
ZIF-67 (211) XRD peak	12.5 deg 2theta	—	—	Text Rounded Reported	article p3 · Results and discussion · Figure 1a
ZIF-67 (422) XRD peak	25 deg 2theta	—	—	Text Rounded Reported	article p3 · Results and discussion · Figure 1a