Porosity — Structures and electrical conductivities of a series of coordination polymers based on tetrathiafulvalene

4 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Complex 1 bulk powdered sample · Powder

Mettler Toledo analyser, 10 deg C/min; plotted in SI Figure S7

Atmosphere: argon in main-text method; SI figure caption says N2
Geometry: Powder
Context: pristine framework
Measurement source: 2, 4 · 2.1 Materials and physical measurements; 3.2 PXRD and TGA · Figure S7

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Solvent-filled channels from TGA	Channels filled with solvent molecules; weight losses cannot be assigned	—	—	Text Qualitative	4 · 3.2 PXRD and TGA · Figure S7
Approximate residual mass at 800 deg C	~41%	—	—	Figure Axis Approximate	S9 · Supplementary Figures · Figure S7

Complex 2 bulk powdered sample · Powder

Mettler Toledo analyser, 10 deg C/min; plotted in SI Figure S7

Atmosphere: argon in main-text method; SI figure caption says N2
Geometry: Powder
Context: pristine framework
Measurement source: 2, 4 · 2.1 Materials and physical measurements; 3.2 PXRD and TGA · Figure S7

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Solvent-filled channels from TGA	Channels filled with solvent molecules; weight losses cannot be assigned	—	—	Text Qualitative	4 · 3.2 PXRD and TGA · Figure S7
Approximate residual mass at 800 deg C	~44%	—	—	Figure Axis Approximate	S9 · Supplementary Figures · Figure S7

Complex 3 bulk powdered sample · Powder

Mettler Toledo analyser, 10 deg C/min; plotted in SI Figure S7

Atmosphere: argon in main-text method; SI figure caption says N2
Geometry: Powder
Context: pristine framework
Measurement source: 2, 4 · 2.1 Materials and physical measurements; 3.2 PXRD and TGA · Figure S7

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Solvent-filled channels from TGA	Channels filled with solvent molecules; weight losses cannot be assigned	—	—	Text Qualitative	4 · 3.2 PXRD and TGA · Figure S7
Approximate residual mass at 800 deg C	~43%	—	—	Figure Axis Approximate	S9 · Supplementary Figures · Figure S7

Complex 3 activated sample · Powder

Activated complex 3 trace plotted in SI Figure S7 under N2 atmosphere; activation details not reported

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Approximate residual mass at 800 deg C	~46%	—	—	Figure Axis Approximate	S9 · Supplementary Figures · Figure S7