Measurement evidence
Atomically Precise Integration of Multiple Functional Motifs in Catalytic Metal-Organic Frameworks for Highly Efficient Nitrate Electroreduction · Lv Y., Su J., Gu Y. et al. · JACS Au · 2022 · 2765-2777
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
As-synthesised In8 red block crystals/powder · Single Crystal
Powdered In8 in 5 mM H2SO4 with 0.5 g L-1 KNO3; selected potentials; room temperature.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TTF radical EPR g value | g = 2.0049 | — | — | Text Exact Reported | main p.4, article p.2768 · Redox-Active Ligands · Fig. 2b |
In8 catalyst ink on carbon paper electrode · Electrode
In8 in pH 1-5 H2SO4/KNO3 electrolytes at selected potentials; 532 nm laser.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| InII Raman peak during reduction | 438 cm^-1 | — | — | Text Exact Reported | main p.5, article p.2769 · pH Dependence · Fig. 2g |
| Initial InIII Raman peaks | 363 and 505 cm^-1 | — | — | Text Exact Reported | main p.4, article p.2768 · pH Dependence · Fig. 2g |
| Adsorbed nitrate Raman band | 806 cm^-1 | — | — | Text Exact Reported | main p.5, article p.2769 · pH Dependence · Fig. 2g |