Other — Iodine uptake enhanced electrical conductivity by a metal-organic framework bearing nanotube array of π-stacked columns

Measurement evidence

Other

Iodine uptake enhanced electrical conductivity by a metal-organic framework bearing nanotube array of π-stacked columns · Chen T., Li S., Wang Z.-B. et al. · Journal of Molecular Structure · 2023 · 135858

2 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

dissolution and recrystallisation regeneration test

regenerated compound 1 crystals · Single Crystal

30.0 mg compound 1 dissolved in 9 mL CH3CN/acetone/DMF (6:2:1 v/v/v) at room temperature and left several days

Context
regenerated pristine compound 1 crystals
Measurement source
3 · 2.3. Regeneration of compound 1 · Fig. 2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
compound 1 regenerated by recrystallisationcrystals of compound 1 can be easily recoveredQualitative
Qualitative
3 · 3.2. Regeneration property · Fig. 2

thermogravimetric analysis

compound 1 crystals · Single Crystal

TG/DTA6300, 10 deg C min^-1, argon stream

Atmosphere
argon
Context
pristine compound 1
Measurement source
2,4 · 2.1; 3.3. IR spectrum and TGA · Fig. S4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
initial solvent-loss mass fraction6.69%0.0669 fractionFigure Axis
Rounded Reported
4 · Supplementary Fig. S4 · Fig. S4
solvent-loss temperature regionbelow 130 deg C403.15 KText
Approximate
4 · 3.3. IR spectrum and TGA · Fig. S4
thermal stability thresholdMarked as a best value within this paperbeyond 150 deg C423.15 KText
Approximate
4 · 3.3. IR spectrum and TGA · Fig. S4