SEM, TEM, SAED, EDX and elemental analysis
Scanning electron microscopyTransmission electron microscopyElemental microanalysis and mappingBulk elemental and compositional analysis
TTF-Pb coordination-polymer microwires · Powder
Microwire precipitate imaged by SEM/TEM; SAED used for phase assessment and EDX/elemental analysis used for composition.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TTF-Pb elemental-analysis composition | 1:1 structure of 1 and Pb(ClO4)2 | — | — | Text Exact Reported | 5126 · Results and Discussion · Figure 1d |
| TTF-Pb microwire isolated yield | Yield: 20.5% (3.6 mg) | — | — | Text Exact Reported | 5129 · Experimental Section |
| TTF-Pb microwire SAED phase assignment | amorphous phase | — | — | Text Qualitative | 5126 · Results and Discussion · Figure 1c |
| TTF-Pb microwire diameter | about 1 um | 1000 nm | — | Text Approximate | 5126 · Results and Discussion · Figure 1 |
| TTF-Pb microwire length | up to several hundreds of microns | — | — | Text Approximate | 5126 · Results and Discussion · Figure 1 |