Diffraction Structure — Two-Dimensional Conductive Ni-HAB as a Catalyst for the Electrochemical Oxygen Reduction Reaction

Measurement evidence

Diffraction Structure

Two-Dimensional Conductive Ni-HAB as a Catalyst for the Electrochemical Oxygen Reduction Reaction · Park J., Chen Z., Flores R.A. et al. · ACS Applied Materials and Interfaces · 2020 · 39074-39081

3 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

PXRD after 0.1 M KOH chemical stability treatment

Cu-HAB powder · Powder

As-synthesised sample suspended in 0.1 M KOH for 24 h at room temperature, washed, dried, degassed and characterised by PXRD.

Temperature
298
Atmosphere
0.1 M KOH aqueous buffer
Geometry
powder
Context
pristine framework powder after chemical treatment
Measurement source
S3 · Section 2. Chemical stability test for Cu-HAB · Figure S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu-HAB PXRD stability after KOHPXRD peak intensity decreased after 0.1 M KOH treatment.Caption
Qualitative
S3 · Figure caption · Figure S2

powder X-ray diffraction (PXRD)

Ni-HAB-H high-crystallinity powder · Powder

Cu-sealed tube, lambda = 1.54 A, capillary, 50 kV and 1 mA; compared before and after 0.1 M KOH buffer treatment.

Geometry
powder in capillary
Context
pristine framework powder
Measurement source
39075-39076; 39078 · Results and Discussion; Experimental Section · Figure 2a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD structure assignment for Ni-HAB-HGood agreement with previously reported 2D honeycomb eclipsed M-HAB structure; PXRD maintained after KOH buffer treatment.Qualitative
Qualitative
39076 · Synthesis of Ni-HAB-H and Ni-HAB-L · Figure 2a

powder X-ray diffraction (PXRD)

Ni-HAB-L low-crystallinity powder · Powder

Cu-sealed tube, lambda = 1.54 A, capillary, 50 kV and 1 mA; compared before and after 0.1 M KOH buffer treatment.

Geometry
powder in capillary
Context
pristine framework powder
Measurement source
39075-39076; 39078 · Results and Discussion; Experimental Section · Figure 2a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD structure assignment for Ni-HAB-LSame Ni-HAB structure as Ni-HAB-H but lower crystallinity; PXRD maintained after KOH buffer treatment.Qualitative
Qualitative
39076 · Synthesis of Ni-HAB-H and Ni-HAB-L · Figure 2a