Microscopy Morphology — Enhanced VOC adsorption capacity on MOF thin layer with reduced particle size by cryogrinding and microwave method

Measurement evidence

Microscopy Morphology

Enhanced VOC adsorption capacity on MOF thin layer with reduced particle size by cryogrinding and microwave method · Gaikwad S., Kim Y., Gaikwad R. et al. · Journal of Environmental Chemical Engineering · 2022 · 107567

2 measurement groups · 20 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM and ImageJ particle-size analysis

All MOF powder samples in paper · Powder

SEM on gold-palladium-coated particles; average crystal size determined with ImageJ.

Context
Pristine MOF powders before and after cryogrinding.
Measurement source
5 · 2.2.7 and Results · Fig. 6; Table 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Average particle size: HKUST-1 - AC3.14 um+/- 0.83 um (SI Table S2)Table
Exact Reported
9 · Results · Table 3
Average particle size: HKUST-1 - BC20.41 um+/- 5.83 um (SI Table S2)Table
Exact Reported
9 · Results · Table 3
Average particle size: MIL-101 - AC0.48 um+/- 0.08 um (SI Table S2)Table
Exact Reported
9 · Results · Table 3
Average particle size: MIL-101 - BC1.38 um+/- 0.53 um (SI Table S2)Table
Exact Reported
9 · Results · Table 3
Average particle size: UiO-66 - AC0.56 um+/- 0.21 um (SI Table S2)Table
Exact Reported
9 · Results · Table 3
Average particle size: UiO-66 - BC0.64 um+/- 0.15 um (SI Table S2)Table
Exact Reported
9 · Results · Table 3
Average particle size: UTSA-16 - microwave - AC2.27 um+/- 0.59 um (SI Table S2)Table
Exact Reported
9 · Results · Table 3
Average particle size: UTSA-16 - microwave - BC5.21 um+/- 2.49 um (SI Table S2)Table
Exact Reported
9 · Results · Table 3
Average particle size: UTSA-16 - solvothermal9.71 um+/- 1.82 um (SI Table S2)Table
Exact Reported
9 · Results · Table 3
Average particle size: ZIF-8Marked as a best value within this paper0.35 um+/- 0.04 um (SI Table S2)Table
Exact Reported
9 · Results · Table 3

SEM/ImageJ individual particle-size statistics

All MOF powder samples in paper · Powder

Ten particle-size measurements per MOF sample with average and standard deviation reported in SI Table S2.

Context
Pristine MOF powders before and after cryogenic grinding.
Measurement source
10-11 · Supporting Information · Table S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Particle-size standard deviation: HKUST-1 - AC+/- 0.83 umSI Table
Exact Reported
10-11 · Supporting Information · Table S2
Particle-size standard deviation: HKUST-1 - BC+/- 5.83 umSI Table
Exact Reported
10-11 · Supporting Information · Table S2
Particle-size standard deviation: MIL-101 - AC+/- 0.08 umSI Table
Exact Reported
10-11 · Supporting Information · Table S2
Particle-size standard deviation: MIL-101 - BC+/- 0.53 umSI Table
Exact Reported
10-11 · Supporting Information · Table S2
Particle-size standard deviation: UiO-66 - AC+/- 0.21 umSI Table
Exact Reported
10-11 · Supporting Information · Table S2
Particle-size standard deviation: UiO-66 - BC+/- 0.15 umSI Table
Exact Reported
10-11 · Supporting Information · Table S2
Particle-size standard deviation: UTSA-16 - microwave - AC+/- 0.59 umSI Table
Exact Reported
10-11 · Supporting Information · Table S2
Particle-size standard deviation: UTSA-16 - microwave - BC+/- 2.49 umSI Table
Exact Reported
10-11 · Supporting Information · Table S2
Particle-size standard deviation: UTSA-16 - solvothermal+/- 1.82 umSI Table
Exact Reported
10-11 · Supporting Information · Table S2
Particle-size standard deviation: ZIF-8+/- 0.04 umSI Table
Exact Reported
10-11 · Supporting Information · Table S2