SEM and ImageJ particle-size analysis
All MOF powder samples in paper · Powder
SEM on gold-palladium-coated particles; average crystal size determined with ImageJ.
- Context
- Pristine MOF powders before and after cryogrinding.
- Measurement source
- 5 · 2.2.7 and Results · Fig. 6; Table 3
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|
| Average particle size: HKUST-1 - AC | 3.14 um | — | +/- 0.83 um (SI Table S2) | Table Exact Reported | 9 · Results · Table 3 |
| Average particle size: HKUST-1 - BC | 20.41 um | — | +/- 5.83 um (SI Table S2) | Table Exact Reported | 9 · Results · Table 3 |
| Average particle size: MIL-101 - AC | 0.48 um | — | +/- 0.08 um (SI Table S2) | Table Exact Reported | 9 · Results · Table 3 |
| Average particle size: MIL-101 - BC | 1.38 um | — | +/- 0.53 um (SI Table S2) | Table Exact Reported | 9 · Results · Table 3 |
| Average particle size: UiO-66 - AC | 0.56 um | — | +/- 0.21 um (SI Table S2) | Table Exact Reported | 9 · Results · Table 3 |
| Average particle size: UiO-66 - BC | 0.64 um | — | +/- 0.15 um (SI Table S2) | Table Exact Reported | 9 · Results · Table 3 |
| Average particle size: UTSA-16 - microwave - AC | 2.27 um | — | +/- 0.59 um (SI Table S2) | Table Exact Reported | 9 · Results · Table 3 |
| Average particle size: UTSA-16 - microwave - BC | 5.21 um | — | +/- 2.49 um (SI Table S2) | Table Exact Reported | 9 · Results · Table 3 |
| Average particle size: UTSA-16 - solvothermal | 9.71 um | — | +/- 1.82 um (SI Table S2) | Table Exact Reported | 9 · Results · Table 3 |
| Average particle size: ZIF-8Marked as a best value within this paper | 0.35 um | — | +/- 0.04 um (SI Table S2) | Table Exact Reported | 9 · Results · Table 3 |
SEM/ImageJ individual particle-size statistics
All MOF powder samples in paper · Powder
Ten particle-size measurements per MOF sample with average and standard deviation reported in SI Table S2.
- Context
- Pristine MOF powders before and after cryogenic grinding.
- Measurement source
- 10-11 · Supporting Information · Table S2
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|
| Particle-size standard deviation: HKUST-1 - AC | +/- 0.83 um | — | — | SI Table Exact Reported | 10-11 · Supporting Information · Table S2 |
| Particle-size standard deviation: HKUST-1 - BC | +/- 5.83 um | — | — | SI Table Exact Reported | 10-11 · Supporting Information · Table S2 |
| Particle-size standard deviation: MIL-101 - AC | +/- 0.08 um | — | — | SI Table Exact Reported | 10-11 · Supporting Information · Table S2 |
| Particle-size standard deviation: MIL-101 - BC | +/- 0.53 um | — | — | SI Table Exact Reported | 10-11 · Supporting Information · Table S2 |
| Particle-size standard deviation: UiO-66 - AC | +/- 0.21 um | — | — | SI Table Exact Reported | 10-11 · Supporting Information · Table S2 |
| Particle-size standard deviation: UiO-66 - BC | +/- 0.15 um | — | — | SI Table Exact Reported | 10-11 · Supporting Information · Table S2 |
| Particle-size standard deviation: UTSA-16 - microwave - AC | +/- 0.59 um | — | — | SI Table Exact Reported | 10-11 · Supporting Information · Table S2 |
| Particle-size standard deviation: UTSA-16 - microwave - BC | +/- 2.49 um | — | — | SI Table Exact Reported | 10-11 · Supporting Information · Table S2 |
| Particle-size standard deviation: UTSA-16 - solvothermal | +/- 1.82 um | — | — | SI Table Exact Reported | 10-11 · Supporting Information · Table S2 |
| Particle-size standard deviation: ZIF-8 | +/- 0.04 um | — | — | SI Table Exact Reported | 10-11 · Supporting Information · Table S2 |