Measurement evidence
Facile synthesis and characterization of trimesic acid-Cu based metal organic frameworks · Sahiner N., Sel K., Ozturk O.F. et al. · Applied Surface Science · 2014 · 663-669
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
TMA-Cu(CH3COOH)2 (DIW) · Powder
0.1 g MOF dissolved in 50 mL 5 M HCl, diluted 100-fold with DI water; triplicate measurements
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu(II) amount | 336.8 +/- 6.8 | — | +/- 6.8 | Table Rounded Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
| Cu(II)/TMA mole ratio | 1.68 | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
TMA-Cu(CH3COOH)2 (EtOH) · Powder
0.1 g MOF dissolved in 50 mL 5 M HCl, diluted 100-fold with DI water; triplicate measurements
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu(II) amount | 321.8 +/- 4.8 | — | +/- 4.8 | Table Rounded Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
| Cu(II)/TMA mole ratio | 1.57 | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
TMA-CuCl2 (DIW) · Powder
0.1 g MOF dissolved in 50 mL 5 M HCl, diluted 100-fold with DI water; triplicate measurements
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu(II) amount | 305.4 +/- 4.6 | — | +/- 4.6 | Table Rounded Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
| Cu(II)/TMA mole ratio | 1.45 | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
TMA-Cu(NO3)2 (DIW) · Powder
0.1 g MOF dissolved in 50 mL 5 M HCl, diluted 100-fold with DI water; triplicate measurements
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu(II) amount | 312.9 +/- 1.0 | — | +/- 1.0 | Table Rounded Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
| Cu(II)/TMA mole ratio | 1.49 | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
TMA-Cu(NO3)2 (EtOH) · Powder
0.1 g MOF dissolved in 50 mL 5 M HCl, diluted 100-fold with DI water; triplicate measurements
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu(II) amount | 364.2 +/- 4.0 | — | +/- 4.0 | Table Rounded Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
| Cu(II)/TMA mole ratio | 1.89 | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
TMA-Cu(SO4)2 (DIW) · Powder
0.1 g MOF dissolved in 50 mL 5 M HCl, diluted 100-fold with DI water; triplicate measurements
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu(II) amount | 315.4 +/- 4.1 | — | +/- 4.1 | Table Rounded Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
| Cu(II)/TMA mole ratio | 1.52 | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
TMA-Cu(SO4)2 (EtOH) · Powder
0.1 g MOF dissolved in 50 mL 5 M HCl, diluted 100-fold with DI water; triplicate measurements
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu(II) amount | 379.7 +/- 2.9 | — | +/- 2.9 | Table Rounded Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
| Cu(II)/TMA mole ratio | 2.03 | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 2 |
TMA-Cu(CH3COOH)2 (DIW) · Powder
3-5 mg sample heated from 50 to 1000 C at 10 C/min under 100 mL/min nitrogen
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TGA degradation step I weight loss | 60-206 C (9.7%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step II weight loss | 269-357 C (44%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step III weight loss | 360-1000 C (59.4%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
TMA-Cu(CH3COOH)2 (EtOH) · Powder
3-5 mg sample heated from 50 to 1000 C at 10 C/min under 100 mL/min nitrogen
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TGA degradation step I weight loss | 263-409 C (50.9%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step II weight loss | 410-1000 C (62.6%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
TMA-CuCl2 (DIW) · Powder
3-5 mg sample heated from 50 to 1000 C at 10 C/min under 100 mL/min nitrogen
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TGA degradation step I weight loss | 88-196 C (6.8%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step II weight loss | 269-366 C (42.5%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step III weight loss | 370-1000 C (56.4%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
TMA-Cu(NO3)2 (DIW) · Powder
3-5 mg sample heated from 50 to 1000 C at 10 C/min under 100 mL/min nitrogen
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TGA degradation step I weight loss | 69-198 C (10.8%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step II weight loss | 277-360 C (64.3%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step III weight loss | 370-1000 C (87.3%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
TMA-Cu(NO3)2 (EtOH) · Powder
3-5 mg sample heated from 50 to 1000 C at 10 C/min under 100 mL/min nitrogen
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TGA degradation step I weight loss | 219-271 C (8.2%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step II weight loss | 312-386 C (17.9%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step III weight loss | 562-722 C (50.8%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step IV weight loss | 811-865 C (54.2%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
TMA-Cu(SO4)2 (DIW) · Powder
3-5 mg sample heated from 50 to 1000 C at 10 C/min under 100 mL/min nitrogen
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TGA degradation step I weight loss | 93-198 C (6.6%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step II weight loss | 269-370 C (41.5%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step III weight loss | 375-1000 C (55.8%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
TMA-Cu(SO4)2 (EtOH) · Powder
3-5 mg sample heated from 50 to 1000 C at 10 C/min under 100 mL/min nitrogen
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| TGA degradation step I weight loss | 224-277 C (8.2%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step II weight loss | 316-376 C (16.9%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step III weight loss | 576-727 C (54.6%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |
| TGA degradation step IV weight loss | 803-876 C (58.7%) | — | — | Table Exact Reported | 5 · 3.2 Structural and thermal analysis · Table 3 |