Synthesis evidence

Fabrication of nonlinear optical metal-organic framework dizinc tetraglycinate dihydrate with optical limiting applications

Bright K.C., Anila R.N., Anugop B. et al. · Journal of Materials Science: Materials in Electronics · 2024 · 2224

1 structured synthesis route

Completeness describes how fully the route could be reconstructed from the main article and supporting information.

Partial recipeSource: Main

Route 1: Other

2 · 2.1 Material synthesis

Metal precursorszinc acetate dihydrate (Sigma-Aldrich ≥ 99.5%)
Linker precursorsglycine (Sigma-Aldrich ≥ 99.5%)
Solventsdouble distilled water
Additivesnone reported
Atmosphereair/ambient, not explicitly specified
Temperature45 for adduct formation; room temperature for evaporation
Time5 h stirring; 30-45 days growth/harvest
Oxidant / reductantnone reported
Work-upheated mixture formed an adduct; adduct redissolved in double distilled water and kept for evaporation; single crystals harvested
Activationnot reported
Scalability contextSlow evaporation over 30-45 days; no yield or batch scale reported.
Show 3 structured reagent records
RoleReagentAmount / concentrationSource
Metal Sourcezinc acetate dihydrate (Sigma-Aldrich ≥ 99.5%)1 part molar ratio2 · 2.1 Material synthesis
Linkerglycine (Sigma-Aldrich ≥ 99.5%)2 parts molar ratio2 · 2.1 Material synthesis
Solventdouble distilled waternot reported2 · 2.1 Material synthesis