Diffraction Structure — Facile design of highly effective Fe-modified bimetallic Fex–Ni1−x-MOFs catalysts with rodlike structures for low-temperature NO reduction by CO

Measurement evidence

Diffraction Structure

Facile design of highly effective Fe-modified bimetallic Fex–Ni1−x-MOFs catalysts with rodlike structures for low-temperature NO reduction by CO · Huang L., Shi Y., Xiong W. et al. · Journal of Materials Science · 2021 · 9914-9928

2 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction

X-ray diffraction and scattering

Fex-Ni1-x-MOF powder catalyst series · Powder

Patterns compared with Ni-MOF and simulated Ni-MOF.

Context: Mixed-metal Fe/Ni MOF series.
Measurement source: 9918-9919 · Catalyst characterizations · Figure 4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
d001 crystallite diameter for Fe0.14-Ni0.86-MOFs	56.8 nm	—	—	Table Exact Reported	9917 · Catalyst characterizations · Table 1
d001 crystallite diameter for Fe0.20-Ni0.80-MOFs	62.4 nm	—	—	Table Exact Reported	9917 · Catalyst characterizations · Table 1
d001 crystallite diameter for Fe0.33-Ni0.67-MOFsMarked as a best value within this paper	63.4 nm	—	—	Table Exact Reported	9917 · Catalyst characterizations · Table 1
d001 crystallite diameter for Fe0.50-Ni0.50-MOFs	52.8 nm	—	—	Table Exact Reported	9917 · Catalyst characterizations · Table 1
Bimetallic framework topology	Diffraction peaks similar to Ni-MOF; same layered topology inferred	—	—	Text Qualitative	9918 · Catalyst characterizations · Figure 4

Powder X-ray diffraction using Rigaku D/Max 2500v/PC with Cu-Ka radiation

X-ray diffraction and scattering

Ni-MOFs · Powder

Cu-Ka radiation, wavelength 0.15406 nm.

Context: Pristine Ni-MOF control.
Measurement source: 9916, 9918 · Characterization; Catalyst characterizations · Figure 4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
d001 crystallite diameter	48.6 nm	—	—	Table Exact Reported	9917 · Catalyst characterizations · Table 1
Main XRD diffraction peak positions	7.3, 11.0, 14.8, 18.4, and 22.5 deg 2theta assigned to (001), (110), (213), (150), and (143)	—	multiple peak positions	Text Rounded Reported	9918 · Catalyst characterizations · Figure 4