Microscopy Morphology — Synthesis, Characterization, and Catalytic Performance of a New Heterobimetallic Y/Tb Metal-Organic Framework with High Catalytic Activity

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Y/Tb-MOF bulk catalyst powder/crystals · Powder

Backscattered FESEM images; elemental mapping for Y and Tb distribution; histogram from 100 particles.

Context: pristine target framework
Measurement source: p004 / 26552 · Synthesis and Characterization of Catalysts · Figure 3; Figure S11

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Y/Tb elemental distribution	uniform distribution of Tb and Y elements	—	—	Text Qualitative	p004 / 26552 · Synthesis and Characterization · Figure 3c,d
SEM particle-size distribution	40 +/- 14	—	+/- 14	Text Rounded Reported	p004 / 26552 · Synthesis and Characterization · Figure S11

Tb-MOF bulk catalyst powder/crystals · Powder

2.5 mg MOF in 5 mL water; stirred, sonicated 1 min, sedimented 5 min; deposited and suspended fractions analysed by ImageJ.

Atmosphere: water
Geometry: optical microscopy
Context: pristine monometallic control
Measurement source: p004 / 26552 · Synthesis and Characterization of Catalysts · Figures S16-S19

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
deposited fraction average size	15 +/- 6	—	+/- 6	Text Rounded Reported	p004 / 26552 · Synthesis and Characterization · Figures S16/S18
suspended fraction average size	11 +/- 4	—	+/- 4	Text Rounded Reported	p004 / 26552 · Synthesis and Characterization · Figures S17/S19

Y/Tb-MOF bulk catalyst powder/crystals · Powder

2.5 mg MOF in 5 mL water; stirred, sonicated 1 min, sedimented 5 min; deposited and suspended fractions analysed by ImageJ.

Atmosphere: water
Geometry: optical microscopy
Context: pristine target framework
Measurement source: p004 / 26552 · Synthesis and Characterization of Catalysts · Figures S14-S15, S18-S19

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
deposited fraction average size	17 +/- 7	—	+/- 7	Text Rounded Reported	p004 / 26552 · Synthesis and Characterization · Figures S14/S18
suspended fraction average size	9 +/- 4	—	+/- 4	Text Rounded Reported	p004 / 26552 · Synthesis and Characterization · Figures S15/S19