Electrochemistry Application — Synthesis and structure of anhydrous Zn2EDTA metal-organic framework

Measurement evidence

Electrochemistry Application

Synthesis and structure of anhydrous Zn2EDTA metal-organic framework · Starodubtseva A.A., Kan T.V., Marshenya S.N. et al. · Polyhedron · 2024 · 116750

4 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Cyclic voltammetry

Zn2EDTA(H2O) comparison electrode · Electrode

Comparison CV in saturated NaClO4 at 10 mV/s, shown in Fig. 5b with Zn2EDTA(H2O) curve.

Geometry
three-electrode cell context
Context
hydrated comparison electrode
Measurement source
p006 / journal page 6 · Results and discussions · Fig. 5b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

Cyclic voltammetry

Zn2EDTA(H2O) comparison electrode · Electrode

Comparison CV in 1 M NaOH at 10 mV/s, shown in Fig. 5a with Zn2EDTA(H2O) curve.

Geometry
three-electrode cell context
Context
hydrated comparison electrode
Measurement source
p006 / journal page 6 · Results and discussions · Fig. 5a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Zn2EDTA(H2O) first-scan anodic peak in 1 M NaOHapproximately +2.0 A/g at approximately -1.43 V vs SCEvisual estimate from plotFigure Axis
Approximate
p006 / journal page 6 · Results and discussions · Fig. 5a

Cyclic voltammetry

Zn2EDTA composite electrode on graphite foil · Electrode

Neutral saturated NaClO4 electrolyte, potential range -1.8 to -0.2 V, sweep rate 10 mV/s; three-electrode cell.

Geometry
three-electrode cell
Context
Zn2EDTA composite electrode with carbon and PVDF
Measurement source
p006 / journal page 6 · Results and discussions · Fig. 5b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Electrolyte pH after working-material dissolutionapproximately pH 2Text
Approximate
p006 / journal page 6 · Results and discussions
Cation intercalation/deintercalation in aqueous solutionimpossible due to high solubilityText
Qualitative
p006-p007 / journal pages 6-7 · Results and discussions; Conclusion
Number of redox peak pairs in saturated NaClO4two pairs of peaksText
Exact Reported
p006 / journal page 6 · Results and discussions · Fig. 5b
Zn2EDTA first-scan main anodic peak in saturated NaClO4approximately +3.6 A/g at approximately -1.36 V vs SCEvisual estimate from plotFigure Axis
Approximate
p006 / journal page 6 · Results and discussions · Fig. 5b
Zn2EDTA first-scan main cathodic peak in saturated NaClO4approximately -8.1 A/g at approximately -1.52 V vs SCEvisual estimate from plotFigure Axis
Approximate
p006 / journal page 6 · Results and discussions · Fig. 5b
Formation constant for protonated Zn-EDTA complexKf = 3.16 x 10^2Text
Exact Reported
p006 / journal page 6 · Results and discussions

Cyclic voltammetry

Zn2EDTA composite electrode on graphite foil · Electrode

Biologic SP-300 potentiostat-galvanostat; three-electrode cell; 1 M NaOH aqueous electrolyte; 10 mV/s sweep; Ag/AgCl (3.5 M KCl) reference; carbon cloth auxiliary.

Geometry
three-electrode cell
Context
Zn2EDTA composite electrode with carbon and PVDF
Measurement source
p003 and p006 / journal pages 3 and 6 · Experimental; Results and discussions · Fig. 5a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Zn2EDTA first-scan anodic peak in 1 M NaOHapproximately +3.4 A/g at approximately -1.40 V vs SCEvisual estimate from plotFigure Axis
Approximate
p006 / journal page 6 · Results and discussions · Fig. 5a
Zn2EDTA first-scan cathodic peak in 1 M NaOHapproximately -4.8 A/g at approximately -1.52 V vs SCEvisual estimate from plotFigure Axis
Approximate
p006 / journal page 6 · Results and discussions · Fig. 5a