Diffraction Structure — Solvent-controlled ion-coupled charge transport in microporous metal chalcogenides

Measurement evidence

Diffraction Structure

Solvent-controlled ion-coupled charge transport in microporous metal chalcogenides · McKenzie J., Kempler P.A., Brozek C.K. · Chemical Science · 2022 · 12747-12759

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

PXRD

TMA2FeGe4S10 microcrystalline powder · Powder

PXRD phase-purity check for TMA2FeGe4S10 and TMA2ZnGe4S10 powders.

Measurement source
SI p.S5 · Synthetic Procedures · Fig. S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Approximate micropore size~1 nm microporesText
Approximate
main p.4, article p.12750 · Results and analysis
PXRD phase purityPhase purity verified by PXRD for TMA2MGe4S10 (M = Zn and Fe)Text
Qualitative
main p.2, article p.12748 · Results and analysis · Fig. S1 and S2

PXRD

TMA4Ge4S10 off-white precursor powder · Powder

Experimental powder XRD compared with simulated TMA4Ge4S10.

Measurement source
SI p.S4 · Synthetic Procedures · Fig. S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD pattern assignmentExperimental PXRD matches simulated TMA4Ge4S10Qualitative
Qualitative
SI p.S4 · Synthetic Procedures · Fig. S1