Porosity — Ionic Liquid-Laden Zn-MOF-74-Based Solid-State Electrolyte for Sodium Batteries

Measurement evidence

Porosity

Ionic Liquid-Laden Zn-MOF-74-Based Solid-State Electrolyte for Sodium Batteries · Mirandona-Olaeta A., Goikolea E., Lanceros-Mendez S. et al. · Batteries · 2023 · 588

2 measurement groups · 14 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

N2 physisorption and BET surface-area analysis

IL0.5@MOF (0.5:1) · Pellet

N2 physisorption at 77 K after vacuum at 100 deg C for 12 h; approximately 100 mg sample; Quantachrome Autosorb-iQ-MP

Temperature
77
Atmosphere
N2
Context
IL0.5@MOF composite compared with pristine Zn-MOF-74
Measurement source
p007 / journal page 7 · 3.1 Physicochemical Characterization · Figure 4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface area of IL0.5@MOF62 m2 g-1Text
Exact Reported
p007 / journal page 7 · 3.1 Physicochemical Characterization · Figure 4
IL0.5@MOF BET fitting relative-pressure range0.068-0.23SI Table
Range
p002 · Supporting information · Table S3
IL0.5@MOF adsorption fitting R20.991SI Table
Exact Reported
p002 · Supporting information · Table S3
IL0.5@MOF external surface area62 m2 g-1SI Table
Exact Reported
p002 · Supporting information · Table S3
IL0.5@MOF micropore surface area0 m2 g-1SI Table
Exact Reported
p002 · Supporting information · Table S3
IL0.5@MOF micropore volume0 cm3 g-1SI Table
Exact Reported
p002 · Supporting information · Table S3
IL0.5@MOF total pore volume0.126 cm3 g-1SI Table
Exact Reported
p002 · Supporting information · Table S3

N2 physisorption and BET surface-area analysis

Zn-MOF-74 powder · Powder

N2 physisorption at 77 K after vacuum at 100 deg C for 12 h; approximately 100 mg sample; Quantachrome Autosorb-iQ-MP

Temperature
77
Atmosphere
N2
Context
pristine Zn-MOF-74 porosity control
Measurement source
p004 / journal page 4 · 2.3 Physicochemical Characterization Techniques · Figure 4; Table S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
BET surface area of pristine Zn-MOF-741123 m2 g-1Text
Exact Reported
p007 / journal page 7 · 3.1 Physicochemical Characterization · Figure 4
Zn-MOF-74 BET fitting relative-pressure range0.007-0.06SI Table
Range
p002 · Supporting information · Table S3
Zn-MOF-74 adsorption fitting R20.9992SI Table
Exact Reported
p002 · Supporting information · Table S3
Zn-MOF-74 external surface area77 m2 g-1SI Table
Exact Reported
p002 · Supporting information · Table S3
Zn-MOF-74 micropore surface area1045 m2 g-1SI Table
Exact Reported
p002 · Supporting information · Table S3
Zn-MOF-74 micropore volume0.384 cm3 g-1SI Table
Exact Reported
p002 · Supporting information · Table S3
Zn-MOF-74 total pore volume0.469 cm3 g-1SI Table
Exact Reported
p002 · Supporting information · Table S3