Diffraction Structure — In-situ growth of electrically conductive MOFs in wood cellulose scaffold for flexible, robust and hydrophobic membranes with improved electrochemical performance

4 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

50%-NiCAT@TOW membrane · Thin Film

WAXS used to quantify cellulose nanofibril alignment retained after NiCAT growth.

Context: composite membrane
Measurement source: p004 / journal page 4 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. 2h-i; Fig. S4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
50%-NiCAT@TOW cellulose orientation factor	0.82	—	—	Text Rounded Reported	p004 / journal page 4 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. S4
cellulose I (110) WAXS scattering peak	~10.9 nm-1	—	~	Text Approximate	p004 / journal page 4 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. 2i
cellulose I (200) WAXS scattering peak	~15.6 nm-1	—	~	Text Approximate	p004 / journal page 4 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. 2i

TOW membrane · Thin Film

Cu K alpha, wavelength 1.5418 A, Eiger2R 1M detector, 100 mm distance, 0.9 mm spot; orientation factor from FWHM.

Context: TOW membrane control
Measurement source: p003 / journal page 3 · 2.4 Materials characterization · Fig. 2g,i; Fig. S4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
TOW cellulose orientation factor	0.89	—	—	Text Rounded Reported	p004 / journal page 4 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. S4

NiCAT powder · Powder

20 kV, 30 mA; NiCAT powder compared with TOW membrane and 50%-NiCAT@TOW.

Context: pristine NiCAT powder control
Measurement source: p003 / journal page 3 · 2.4 Materials characterization · Fig. 3a

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
NiCAT (002) XRD peak	2theta = 27.5 deg	—	—	Text Rounded Reported	p005 / journal page 5 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. 3a
NiCAT (100) XRD peak	2theta = 4.6 deg	—	—	Text Rounded Reported	p005 / journal page 5 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. 3a
NiCAT (200) XRD peak	2theta = 9.4 deg	—	—	Text Rounded Reported	p005 / journal page 5 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. 3a
NiCAT (210) XRD peak	2theta = 12.5 deg	—	—	Text Rounded Reported	p005 / journal page 5 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. 3a

50%-NiCAT@TOW membrane · Thin Film

XRD pattern of 50%-NiCAT@TOW membrane used to confirm NiCAT integration with cellulose crystalline faces.

Context: composite membrane
Measurement source: p005 / journal page 5 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. 3a

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
NiCAT integration in 50%-NiCAT@TOW	XRD shows cellulose (101)/(200) and NiCAT (100)/(200)/(210)/(002) peaks	—	—	Qualitative Qualitative	p005 / journal page 5 · 3.1 Preparation of EC-MOF@TOW membrane · Fig. 3a