Diffraction Structure — Diamagnetic Carrier-Doping-Induced Continuous Electronic and Magnetic Crossover in One-Dimensional Coordination Polymers

Measurement evidence

Diffraction Structure

Diamagnetic Carrier-Doping-Induced Continuous Electronic and Magnetic Crossover in One-Dimensional Coordination Polymers · Shen Y., Cui M., Li G. et al. · Journal of the American Chemical Society · 2024 · 35367-35376

2 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction (PXRD), theta-2theta scan, Cu Kalpha radiation

X-ray diffraction and scattering

all Cu-doping-ratio powders · Powder

Measured in air; PXRD patterns compared across x = 0 to 1.

Atmosphere: air
Context: Series-wide structural comparison
Measurement source: 8 · Experimental Section · Figure 1b

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PXRD retained after Cu doping	PXRD patterns remain consistent with undoped Cu0.0Co1.0 after Cu doping	—	—	Text Qualitative	2 · Synthesis of the 1D Coordination Polymers · Figure 1b

PXRD indexing, Pawley refinement, simulated annealing and Rietveld refinement

X-ray diffraction and scattering

Cu0.0Co1.0 · Powder

Cu0.0Co1.0 crystal structure solved/refined from powder diffraction.

Context: Pristine Co end-member
Measurement source: 2 · Supporting Information · Figure S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Cu0.0Co1.0 Rietveld Rwp	Rwp = 8.55%	—	—	SI Table Exact Reported	2 · Figure S1 text · Figure S1
Cu0.0Co1.0 Rietveld cell a	a = 11.60228 Angstrom	—	—	SI Table Exact Reported	2 · Figure S1 text · Figure S1
Cu0.0Co1.0 Rietveld cell b	b = 9.09867 Angstrom	—	—	SI Table Exact Reported	2 · Figure S1 text · Figure S1
Cu0.0Co1.0 Rietveld cell c	c = 17.05542 Angstrom	—	—	SI Table Exact Reported	2 · Figure S1 text · Figure S1
Cu0.0Co1.0 Rietveld cell volume	V = 1631.754 Angstrom^3	—	—	SI Table Exact Reported	2 · Figure S1 text · Figure S1
Cu0.0Co1.0 space group	Triclinic P1	—	—	SI Table Exact Reported	2 · Figure S1 text · Figure S1