Measurement evidence
Alkali-metal-regulated construction of superhydrophilic ZnII and CdII coordination polymers with perhalogenated terephthalate ligands · Chen S.-C., Zhang Z.-H., Huang K.-L. et al. · CrystEngComm · 2013 · 9613-9622
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Complex 1 colourless crystals · Single Crystal
reported approximate solubility in water
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| water solubility | ca. 145 mg mL^-1 | — | ca. | Text Approximate | p003 · Syntheses and solution characterization |
Complex 2 colourless crystals · Single Crystal
reported approximate solubility in water
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| water solubility | ca. 170 mg mL^-1 | — | ca. | Text Approximate | p003 · Syntheses and solution characterization |
Complex 3 colourless crystals · Single Crystal
reported approximate solubility in water
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| water solubility | ca. 180 mg mL^-1 | — | ca. | Text Approximate | p003 · Syntheses and solution characterization |
Complex 4 colourless crystals · Single Crystal
reported approximate solubility in water
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| water solubility | ca. 165 mg mL^-1 | — | ca. | Text Approximate | p003 · Syntheses and solution characterization |
Complex 5 colourless crystals · Single Crystal
reported approximate solubility in water
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| water solubilityMarked as a best value within this paper | ca. 285 mg mL^-1 | — | ca. | Text Approximate | p003 · Syntheses and solution characterization |
Complex 6 colourless crystals · Single Crystal
reported approximate solubility in water
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| water solubility | ca. 260 mg mL^-1 | — | ca. | Text Approximate | p003 · Syntheses and solution characterization |
Complex 1 colourless crystals · Single Crystal
heated from 20 to 800 deg C at 10 deg C min-1
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| first mass loss | 13.24% from 110-170 deg C; calculated 13.89%; assigned six coordinated methanol molecules | — | — | Text Exact Reported | p009 · Thermogravimetric analysis · Fig. S9 |
Complex 2 colourless crystals · Single Crystal
heated from 20 to 800 deg C at 10 deg C min-1
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| DMF ligand mass loss | 27.03% from 115-220 deg C; calculated 27.55% | — | — | Text Exact Reported | p009 · Thermogravimetric analysis · Fig. S9 |
| coordinated water mass loss | 6.31% from 60-110 deg C; calculated 6.78% | — | — | Text Exact Reported | p009 · Thermogravimetric analysis · Fig. S9 |
Complex 3 colourless crystals · Single Crystal
heated from 20 to 800 deg C at 10 deg C min-1
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| thermal stability onset | stable up to 140 deg C; begins to decompose at ca. 490 deg C | — | ca. 490 deg C decomposition | Text Approximate | p009 · Thermogravimetric analysis · Fig. S9 |
Complex 4 colourless crystals · Single Crystal
heated from 20 to 800 deg C at 10 deg C min-1
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| first mass loss | 16.82% from 95-270 deg C; calculated 17.49%; assigned coordinated DMF and Me2NH | — | — | Text Exact Reported | p009 · Thermogravimetric analysis · Fig. S9 |
Complex 5 colourless crystals · Single Crystal
heated from 20 to 800 deg C at 10 deg C min-1
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| water mass loss | 15.18% below 155 deg C; calculated 14.84%; assigned all water molecules | — | — | Text Exact Reported | p009 · Thermogravimetric analysis · Fig. S9 |
Complex 6 colourless crystals · Single Crystal
heated from 20 to 800 deg C at 10 deg C min-1
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| water mass lossMarked as a best value within this paper | 33.49% from 50-200 deg C; calculated 32.91%; assigned six coordinated and four lattice waters | — | — | Text Exact Reported | p009 · Thermogravimetric analysis · Fig. S9 |