Diffraction Structure — Pillared nickel-based metal-organic frameworks as electrode material with high electrochemical performance

Measurement evidence

Diffraction Structure

Pillared nickel-based metal-organic frameworks as electrode material with high electrochemical performance · Jiang X., Deng S., Sun L. et al. · Journal of Electroanalytical Chemistry · 2020 · 114802

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction with Cu Kalpha radiation

X-ray diffraction and scattering

(Zn/Ni)2(bdc)2P powder · Powder

X'Pert Pro diffractometer; lambda = 1.5406 A; scan step 0.02 deg in 2theta; comparison to simulated single-crystal patterns.

Geometry: powder
Context: Pristine Ni2(bdc)2P, Zn2(bdc)2P and mixed-metal (Zn/Ni)2(bdc)2P powders.
Measurement source: 2-3 · 2.2 Characterization; 3.1 Structure characterization · Fig. 2a,b

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ni2(bdc)2P XRD phase match	XRD patterns of synthesized Ni2(bdc)2P match well with simulated [Ni2(BDC)2(DABCO)] framework.	—	—	Text Qualitative	3 · 3.1 Structure characterization · Fig. 2a
(Zn/Ni)2(bdc)2P XRD peak shift	Diffraction peaks shift toward larger angle compared with Ni2(bdc)2P, indicating Zn2+ partially replaced Ni2+.	—	—	Text Qualitative	3 · 3.1 Structure characterization · Fig. 2b

Powder X-ray diffraction pattern for Zn2(bdc)2P

X-ray diffraction and scattering

Zn2(bdc)2P powder · Powder

Experimental Zn2(bdc)2P XRD compared with simulated pattern in Supplementary Fig. S1.

Geometry: powder
Context: Pristine Zn2(bdc)2P framework control.
Measurement source: SI p.1 · Supplementary Materials · Fig. S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Zn2(bdc)2P XRD experimental/simulation match	Experimental Zn2(bdc)2P XRD pattern shown against simulation; main text identifies it as simulated from CCDC 238859.	—	—	Caption Qualitative	SI p.1 · Supplementary Materials · Fig. S1