Microscopy Morphology — Pillared nickel-based metal-organic frameworks as electrode material with high electrochemical performance

Measurement evidence

Microscopy Morphology

Pillared nickel-based metal-organic frameworks as electrode material with high electrochemical performance · Jiang X., Deng S., Sun L. et al. · Journal of Electroanalytical Chemistry · 2020 · 114802

1 measurement group · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FESEM with EDS elemental mapping

Scanning electron microscopy Elemental microanalysis and mapping

(Zn/Ni)2(bdc)2P powder · Powder

Zeiss SIGMA FESEM; EDS maps and spectrum for (Zn/Ni)2(bdc)2P.

Geometry: powder microcrystals
Context: Pristine M2(bdc)2P powder series.
Measurement source: 2,5-6 · 2.2 Characterization; 3.1 Structure characterization · Fig. 4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
(Zn/Ni)2(bdc)2P EDS elemental distribution	Ni, C, O and N uniformly distributed; Zn weak/not obvious due to low Zn2+ content; EDS spectrum verifies Zn.	—	—	Text Qualitative	5 · 3.1 Structure characterization · Fig. 4g,h
Ni2(bdc)2P cuboid length	about 2 um to 20 um	—	range 2-20 um	Text Range	5 · 3.1 Structure characterization · Fig. 4a,d
Zn2(bdc)2P layer thickness	around 500 nm	—	—	Text Approximate	5 · 3.1 Structure characterization · Fig. 4b,e
(Zn/Ni)2(bdc)2P cuboid length	about 2 um to 20 um	—	range 2-20 um	Text Range	5 · 3.1 Structure characterization · Fig. 4c,f
Supplementary Ni2(bdc)2P FESEM length labels	4, 8, 11 and 14 um labelled on low-magnification FESEM image	—	multiple labelled dimensions	Figure Axis Approximate	SI p.2 · Supplementary Materials · Fig. S2
Supplementary (Zn/Ni)2(bdc)2P FESEM length labels	3, 8, 9, 20 and 22 um labelled on low-magnification FESEM image	—	multiple labelled dimensions	Figure Axis Approximate	SI p.2 · Supplementary Materials · Fig. S2