Other — A novel lamella 2D Ag(I) coordination polymer of graphite-like structure featuring short interlayer distance

Measurement evidence

Other

A novel lamella 2D Ag(I) coordination polymer of graphite-like structure featuring short interlayer distance · Sun D., Luo G.-G., Xu Q.-J. et al. · Inorganic Chemistry Communications · 2009 · 782-784

2 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Elemental analysis

Pale yellow block crystals of 1 · Single Crystal

CE instruments EA 1110 analyser for C, H and N contents.

Context
pristine target framework
Measurement source
2 · Experimental Procedures
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Calculated carbon contentC 28.11%Text
Exact Reported
3 · Reference 8
Found carbon contentMarked as a best value within this paperC 28.15%Text
Exact Reported
3 · Reference 8
Found hydrogen contentMarked as a best value within this paperH 3.01%Text
Exact Reported
3 · Reference 8
Found nitrogen contentMarked as a best value within this paperN 14.03%Text
Exact Reported
3 · Reference 8

TGA-DSC

Bulk powder/crystalline solid of 1 · Powder

Measured from 30 to 800 degC on an SDT Q600 under nitrogen gas flow of 5 ml/min.

Atmosphere
nitrogen, 5 ml/min
Context
pristine target framework
Measurement source
2 · Experimental Procedures · Fig. S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Approximate residual mass at 800 degCca. 42% residual mass at 800 degCca.Visual Estimate
Approximate
4 · Fig. S3 · Fig. S3
Lattice water count confirmationTGA confirms the number of lattice water molecules; formula contains 9 H2OText
Qualitative
2 · Crystal packing discussion · Fig. S3
Early TGA mass loss labelled in SIMarked as a best value within this paper9.1% labelled mass lossFigure Axis
Approximate
4 · Fig. S3 · Fig. S3