Diffraction Structure — Zinc terephthalates ZnC8H4O4 as anodes for lithium ion batteries

Measurement evidence

Diffraction Structure

Zinc terephthalates ZnC8H4O4 as anodes for lithium ion batteries · Wang L., Zou J., Chen S. et al. · Electrochimica Acta · 2017 · 304-310

3 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

X-ray powder diffraction

amorphous ZnTPA powder (ZnTPA-amor) · Powder

Cu Kalpha radiation, lambda = 1.54056 A, step size 0.03 deg.

Geometry
powder
Context
pristine amorphous ZnTPA phase
Measurement source
305 · Results and discussion · Fig. 1b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Amorphous ZnTPA phase assignmentquasi-amorphous phase with no carbon indicated by XRD/RamanText
Qualitative
305 · Results and discussion · Fig. 1b

X-ray powder diffraction

well-crystalline anhydrous ZnTPA powder · Powder

Cu Kalpha radiation, lambda = 1.54056 A, step size 0.03 deg.

Geometry
powder
Context
pristine crystalline ZnTPA phase
Measurement source
305 · Results and discussion · Fig. 1b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Crystalline ZnTPA phase after 300 deg C annealanhydrous ZnTPA obtained with good crystallineText
Qualitative
305 · Results and discussion · Fig. 1b

X-ray powder diffraction and Rietveld refinement

as-synthesised ZnTPA.2H2O powder · Powder

Cu Kalpha radiation, lambda = 1.54056 A, step size 0.03 deg.

Geometry
powder
Context
pristine hydrated ZnTPA phase
Measurement source
305-306 · 2.2 Materials characterization; Results and discussion · Fig. 1b-d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
ZnTPA.2H2O longer carboxylate C-O bond length1.289 AText
Exact Reported
306 · Results and discussion · Fig. 1d
ZnTPA.2H2O shorter carboxylate C-O bond length1.2730 AText
Exact Reported
306 · Results and discussion · Fig. 1d
ZnTPA.2H2O inorganic layer distance7.50 AText
Exact Reported
305 · Results and discussion · Fig. 1c
ZnTPA.2H2O organic layer distance6.10 AText
Exact Reported
305 · Results and discussion · Fig. 1c
ZnTPA.2H2O beta anglebeta = 103.82 degText
Exact Reported
305 · Results and discussion · Fig. 1b
ZnTPA.2H2O lattice parameter aa = 14.922 AText
Exact Reported
305 · Results and discussion · Fig. 1b
ZnTPA.2H2O lattice parameter bb = 5.030 AText
Exact Reported
305 · Results and discussion · Fig. 1b
ZnTPA.2H2O lattice parameter cc = 12.098 AText
Exact Reported
305 · Results and discussion · Fig. 1b
ZnTPA.2H2O phase and space grouppure phase with C2/c space groupText
Qualitative
305 · Results and discussion · Fig. 1b