Complete recipeSource: SI
Route 1: Solvothermal
SI p.2 · Preparation of conductive Ni-MOF
Metal precursorsNickel acetate tetrahydrate (Ni(OAc)2.4H2O), 0.04 mmol
Linker precursorsHHTP, 0.02 mmol
Solvents1 mL water/DMF solvent mixture, v:v = 1:1
AtmosphereNot specified
Temperature85
Time15
Work-upCool to room temperature; centrifuge; wash solid precipitate with ultrapure water and alcohol.
ActivationDried overnight under vacuum at 75 C.
Scalability contextSmall-vial batch: 20 mL glass vial, 1 mL solvent mixture; no scale-up data reported.
Show 3 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Linker | HHTP | 0.02 mmol | SI p.2 · Preparation of conductive Ni-MOF |
| Metal Source | Ni(OAc)2.4H2O | 0.04 mmol | SI p.2 · Preparation of conductive Ni-MOF |
| Solvent | water/DMF (v:v = 1:1) | 1 mL | SI p.2 · Preparation of conductive Ni-MOF |