Diffraction Structure — Si nanoparticles confined within a conductive 2D porous Cu-based metal–organic framework (Cu3(HITP)2) as potential anodes for high-capacity Li-ion batteries

Measurement evidence

Diffraction Structure

Si nanoparticles confined within a conductive 2D porous Cu-based metal–organic framework (Cu3(HITP)2) as potential anodes for high-capacity Li-ion batteries · Nazir A., Le H.T.T., Kasbe A. et al. · Chemical Engineering Journal · 2021 · 126963

2 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

X-ray powder diffraction, D/MAX Ultima III

X-ray diffraction and scattering

Si@Cu3(HITP)2-5 · Powder

XRD patterns for pure Si and Si@Cu3(HITP)2-5/10/15 composites.

Geometry: powder
Context: Composite plus pure Si control
Measurement source: 4 · Results and discussion · Fig. 1a

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Composite XRD phase assignment	All composite XRD patterns indexed to cubic Si (JCPDS 27-1402) without impurity phase; Cu3(HITP)2 feature peaks not observed.	—	—	Qualitative Qualitative	4 · Results and discussion · Fig. 1a

X-ray powder diffraction, D/MAX Ultima III

X-ray diffraction and scattering

pure Cu-MOF (Cu3(HITP)2) · Powder

Phase identification and purity of pure Cu3(HITP)2.

Geometry: powder
Context: Pristine Cu-MOF control
Measurement source: 4 · Results and discussion · Fig. S1a

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Cu3(HITP)2 unit cell a	a = 22.3 A	—	—	Text Rounded Reported	4 · Results and discussion
Cu3(HITP)2 unit cell b	b = 22.3 A	—	—	Text Rounded Reported	4 · Results and discussion
Cu3(HITP)2 unit cell c	c = 27.8 A	—	—	Text Rounded Reported	4 · Results and discussion
Cu3(HITP)2 XRD (001) peak	2theta = 27.8 deg	—	—	Text Rounded Reported	4 · Results and discussion · Fig. S1a
Cu3(HITP)2 XRD (100) peak	2theta = 4.9 deg	—	—	Text Rounded Reported	4 · Results and discussion · Fig. S1a
Cu3(HITP)2 XRD (200) peak	2theta = 9.7 deg	—	—	Text Rounded Reported	4 · Results and discussion · Fig. S1a