cMOF Evidence Base
Microscopy Morphology — Overcoming Diffusion Limitation of Faradaic Processes: Property-Performance Relationships of 2D Conductive Metal-Organic Framework Cu3(HHTP)2 for Reversible Lithium-Ion Storage

Measurement evidence

Microscopy Morphology

Overcoming Diffusion Limitation of Faradaic Processes: Property-Performance Relationships of 2D Conductive Metal-Organic Framework Cu3(HHTP)2 for Reversible Lithium-Ion Storage · Wrogemann J.M., Luther M.J., Barmann P. et al. · Angewandte Chemie - International Edition · 2023 · e202303111

3 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM-EDX elemental analysis

Scanning electron microscopyElemental microanalysis and mappingBulk elemental and compositional analysis

Flake-like Cu3(HHTP)2 powder activated at 60 C · Powder

ZEISS Gemini SEM; EDX at 15 kV using Oxford Instruments X-Max; samples gold-coated briefly to avoid charging.

Atmosphere
ambient for SEM/EDX preparation
Geometry
powder on adhesive carbon tabs
Context
pristine powder
Measurement source
S-9 · 2.1 · Table S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Flake-like Cu3(HHTP)2 carbon atomic fraction71.33 +/- 0.52 at%—+/- 0.52 at%SI Table
Exact Reported		S-9 · 2.1 · Table S1
Flake-like Cu3(HHTP)2 copper atomic fraction7.0 +/- 0.88 at%—+/- 0.88 at%SI Table
Exact Reported		S-9 · 2.1 · Table S1
Flake-like Cu3(HHTP)2 oxygen atomic fraction21.68 +/- 1.27 at%—+/- 1.27 at%SI Table
Exact Reported		S-9 · 2.1 · Table S1

SEM-EDX elemental analysis

Scanning electron microscopyElemental microanalysis and mappingBulk elemental and compositional analysis

Rod-like Cu3(HHTP)2 powder activated at 60 C · Powder

ZEISS Gemini SEM; EDX at 15 kV using Oxford Instruments X-Max; samples gold-coated briefly to avoid charging.

Atmosphere
ambient for SEM/EDX preparation
Geometry
powder on adhesive carbon tabs
Context
pristine powder
Measurement source
S-3 and S-9 · 1.2.1; 2.1 · Table S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Rod-like Cu3(HHTP)2 carbon atomic fraction69.87 +/- 0.26 at%—+/- 0.26 at%SI Table
Exact Reported		S-9 · 2.1 · Table S1
Rod-like Cu3(HHTP)2 copper atomic fraction5.87 +/- 0.46 at%—+/- 0.46 at%SI Table
Exact Reported		S-9 · 2.1 · Table S1
Rod-like Cu3(HHTP)2 oxygen atomic fraction24.26 +/- 0.67 at%—+/- 0.67 at%SI Table
Exact Reported		S-9 · 2.1 · Table S1

Scanning electron microscopy

Scanning electron microscopy

Rod-like Cu3(HHTP)2 powder activated at 60 C · Powder

SEM at 3 kV InLens detector; compared rod-like and flake-like synthesized products.

Geometry
powder morphology
Context
pristine powder comparison
Measurement source
p003 · Results and Discussion · Figure 1a,b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Flake-like morphologynanometre-thin flake-like particles——Text
Qualitative		p004 · Results and Discussion · Figure 1b
Rod-like morphologyrod-like particles of several micrometres in length——Text
Qualitative		p004 · Results and Discussion · Figure 1a