Microscopy Morphology — Synthetic Routes for a 2D Semiconductive Copper Hexahydroxybenzene Metal-Organic Framework

Measurement evidence

Microscopy Morphology

Synthetic Routes for a 2D Semiconductive Copper Hexahydroxybenzene Metal-Organic Framework · Park J., Hinckley A.C., Huang Z. et al. · Journal of the American Chemical Society · 2018 · 14533-14537

1 measurement group · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

HRTEM/TEM at 200 kV

Transmission electron microscopy

Cu-HHB H2O 60 C post-treated powder · Powder

HRTEM along [001] and TEM images; JEOL JEM2100 at 200 kV according to SI instrumentation.

Atmosphere: High-vacuum TEM environment, not further specified
Geometry: Powder/nanosheet TEM sample
Context: Pristine Cu-HHB powder morphology and lattice imaging
Measurement source: p002 · Main text · Figure 2a; Figure S4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Observed HRTEM d020 spacing	d020 = 10.9 A	—	—	Text Rounded Reported	p002-p003 · Main text · Figure 2a
Observed HRTEM d110 spacing	d110 = 11.7 A	—	—	Text Rounded Reported	p002-p003 · Main text · Figure 2a