Other — Conductive metal-organic frameworks with wheel-shaped metallomacrocycle subunits as high-performance supercapacitor electrodes

Measurement evidence

Other

Conductive metal-organic frameworks with wheel-shaped metallomacrocycle subunits as high-performance supercapacitor electrodes · Yan Y., Lin X., Ge J. et al. · Chemical Engineering Journal · 2023 · 143739

2 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SQUID magnetic susceptibility and AC susceptibility

MWM-1 (Co/2Ni) powder/crystals · Powder

Quantum Design MPMS 6000; temperature and frequency dependent susceptibility, 0 and 1000 Oe DC fields

Temperature
1.8-300
Geometry
powder
Context
pristine target and pristine control
Measurement source
6-7 · Section 3.2 · Fig. 4; Supplementary Fig. S10-S12
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
molar susceptibility/spin-state increaseincreased nearly by a factor of fournearlyText
Approximate
7 · Section 3.2 · Fig. 4

thermogravimetric analysis (TGA)

MWM-1 (Co) powder/crystals · Powder

25-800 C under N2, heating rate 5 C min-1

Temperature
298-1073
Atmosphere
N2
Geometry
powder
Context
pristine target and control thermal stability
Measurement source
S1-S10 · Figure S6 caption and text · Figure S6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TGA stage 1 mass lossabout 3.60% from 30 to 200 CaboutText
Approximate
S1-S10 · Figure S6 text · Figure S6
TGA stage 2 mass lossabout 4.70% from 200 to 305 CaboutText
Approximate
S1-S10 · Figure S6 text · Figure S6
TGA stage 3 mass loss~59.66% from 305 to 424 C~Text
Approximate
S1-S10 · Figure S6 text · Figure S6