Other — Co-Ca Phosphonate Showing Humidity-Sensitive Single Crystal to Single Crystal Structural Transformation and Tunable Proton Conduction Properties

Measurement evidence

Other

Co-Ca Phosphonate Showing Humidity-Sensitive Single Crystal to Single Crystal Structural Transformation and Tunable Proton Conduction Properties · Bao S.-S., Li N.-Z., Taylor J.M. et al. · Chemistry of Materials · 2015 · 8116-8125

1 measurement group · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Thermogravimetric analysis

Fresh violet sheet-like CoCa.4H2O crystals · Single Crystal

Thermogravimetric curves of CoCa.4H2O and CoCa.2H2O under nitrogen.

Temperature
298-1073 K
Atmosphere
Nitrogen gas flow
Context
pristine framework hydrated phases
Measurement source
main p.4, article p.8119 · Thermal Stability · Figure 2a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
CoCa.2H2O dehydration weight loss below 200 Cobserved weight loss = 10.9%; calculated = 10.6%Text
Rounded Reported
main p.4, article p.8119 · Thermal Stability · Figure 2a
CoCa.4H2O dehydration weight loss below 200 Cobserved total weight loss = 14.8%; calculated = 15.1%Text
Rounded Reported
main p.4, article p.8119 · Thermal Stability · Figure 2a
Framework decomposition onset after dehydration plateauplateau between 200 and 275 C; above this organic components decomposed and structures collapseText
Rounded Reported
main p.4, article p.8119 · Thermal Stability · Figure 2a