Measurement evidence
Electrically conductive Pt-MOFs for acidic oxygen reduction: Optimized performance via altering conjugated ligands · Iqbal R., Ali S., Saleem A. et al. · Chemical Engineering Journal · 2023 · 140799
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Pt3(C12N6O6)2 MOF thin film on Si · Thin Film
2D GIXD spectrum of Pt3(C12N6O6)2 MOF thin film on Si.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| 2D sheet orientation | mainly face-on orientation; [100] in plane Qz~0 and [002] near meridian Qxy~0 | — | — | Qualitative Qualitative | p. 4 · 3.1 · Fig. 3a |
Pt3(C12N9H3O3)2 MOF black powder · Powder
Rigaku RINT Ultima III; Pawley refinement using Reflex in MS modelling.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| [002] broad peak position | 27.92 degrees | — | — | Text Exact Reported | p. 5 · 3.1 · Fig. 2 |
| [100] XRD peak position | 5.61 degrees | — | — | Text Exact Reported | p. 4 · 3.1 · Fig. 2 |
| lattice parameter a | a = 21.56 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| lattice parameter b | b = 21.50 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| lattice parameter c / d-spacing | c = 3.12 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| metal-metal distance Dm | 10.73 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| pore size DpMarked as a best value within this paper | 17.18 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| RP refinement value | 3.39 | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| RWP refinement valueMarked as a best value within this paper | 2.19 | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
Pt3(C12N12H6)2 MOF black powder · Powder
Rigaku RINT Ultima III; Pawley refinement using Reflex in MS modelling.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| [002] broad peak position | 26.32 degrees | — | — | Text Exact Reported | p. 5 · 3.1 · Fig. 2 |
| [100] XRD peak position | 5.54 degrees | — | — | Text Exact Reported | p. 4 · 3.1 · Fig. 2 |
| lattice parameter a | a = 21.82 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| lattice parameter b | b = 21.87 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| lattice parameter c / d-spacing | c = 3.33 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| metal-metal distance Dm | 10.93 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| pore size Dp | 14.48 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| RP refinement value | 2.85 | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| RWP refinement value | 2.78 | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
Pt3(C12N6O6)2 MOF black powder · Powder
Rigaku RINT Ultima III; Pawley refinement using Reflex in MS modelling.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| [002] broad peak position | 28.16 degrees | — | — | Text Exact Reported | p. 5 · 3.1 · Fig. 2 |
| [100] XRD peak position | 5.63 degrees | — | — | Text Exact Reported | p. 4 · 3.1 · Fig. 2 |
| lattice parameter a | a = 21.99 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| lattice parameter b | b = 21.99 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| lattice parameter c / d-spacing | c = 3.09 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1; Fig. 3b |
| metal-metal distance Dm | 10.76 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| pore size Dp | 14.10 A | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| RP refinement value | 3.12 | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |
| RWP refinement value | 2.45 | — | — | Table Exact Reported | p. 5 · 3.1 · Table 1 |