EXAFS, XANES and XPS
Pt3(C12N6O6)2 MOF black powder · Powder
Pt L3-edge XAS and Pt 4f XPS used to assign Pt-O coordination and Pt2+ state.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| EXAFS fitted Pt-O bond distance | 1.92 A | — | — | SI Table Exact Reported | p. 28 · EXAFS Spectrum Fitting · Table S12 |
| EXAFS fitted Pt-O coordination number | 3.8 | — | — | SI Table Exact Reported | p. 28 · EXAFS Spectrum Fitting · Table S12 |
| EXAFS inner potential correction DeltaE0 | 0.8 eV | — | — | SI Table Exact Reported | p. 28 · EXAFS Spectrum Fitting · Table S12 |
| EXAFS R factor | 0.0095 | — | — | SI Table Exact Reported | p. 28 · EXAFS Spectrum Fitting · Table S12 |
| EXAFS Debye-Waller factor | 0.0125 A^2 | — | — | SI Table Exact Reported | p. 28 · EXAFS Spectrum Fitting · Table S12 |
| FT-EXAFS main peak | 1.61 A | — | — | Text Exact Reported | p. 4 · 3.1 · Fig. 3c |
| FT-EXAFS additional peak | 2.6 A | — | — | Text Rounded Reported | p. 4 · 3.1 · Fig. 3c |
| Pt L3-edge XANES peak | 11566.8 eV | — | — | Text Exact Reported | p. 5 · 3.1 · Fig. 3d |
| Pt 4f5/2 binding energy | 76.1 eV | — | — | Text Exact Reported | p. 5 · 3.1 · Fig. S4 |
| Pt 4f7/2 binding energy | 72.8 eV | — | — | Text Exact Reported | p. 5 · 3.1 · Fig. S4 |