Microscopy Morphology — Operando Elucidation of Electrocatalytic and Redox Mechanisms on a 2D Metal Organic Framework Catalyst for Efficient Electrosynthesis of Hydrogen Peroxide in Neutral Media

Measurement evidence

Microscopy Morphology

Operando Elucidation of Electrocatalytic and Redox Mechanisms on a 2D Metal Organic Framework Catalyst for Efficient Electrosynthesis of Hydrogen Peroxide in Neutral Media · Ross R.D., Sheng H., Ding Y. et al. · Journal of the American Chemical Society · 2022 · 15845-15854

2 measurement groups · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM

Ni-HAB powder · Powder

Nanoscale Ni-HAB powder imaged on carbon tape; 1 kV imaging and 17 kV EDS method reported in SI.

Context
pristine framework
Measurement source
15846 · Results · Figure 1b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

TEM

Ni-HAB powder · Powder

Dispersed Ni-HAB on lacey carbon TEM grids; (100) plane spacing labelled.

Context
pristine framework
Measurement source
15847 · Results · Figure 1c
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Observed Ni-HAB (100) plane spacing1.18 nm average distance between (100) planesText
Rounded Reported
15847 · Results · Figure 1c
Expected Ni-HAB (100) plane spacing1.20 nm expected (100) plane spacingText
Rounded Reported
15847 · Results · Figure 1c